data_01 _audit_creation_date 2017-08-03 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.07.20 svn.r3457 for OlexSys, GUI svn.r5370) ; _shelx_SHELXL_version_number '2014/7' _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_id_orcid ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '4(C24 H17 F3 N2 O), C4 H10 O' _chemical_formula_sum 'C100 H78 F12 N8 O5' _chemical_formula_weight 1699.70 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.3304(12) _cell_length_b 17.890(2) _cell_length_c 23.784(3) _cell_angle_alpha 96.034(5) _cell_angle_beta 99.172(5) _cell_angle_gamma 99.186(5) _cell_volume 4245.1(9) _cell_formula_units_Z 2 _cell_measurement_reflns_used 9992 _cell_measurement_temperature 291(2) _cell_measurement_theta_max 26.66 _cell_measurement_theta_min 2.33 _shelx_estimated_absorpt_T_max 0.986 _shelx_estimated_absorpt_T_min 0.975 _exptl_absorpt_coefficient_mu 0.101 _exptl_absorpt_correction_T_max ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_type 'none' _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.330 _exptl_crystal_density_meas . _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1764 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.14 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0906 _diffrn_reflns_av_unetI/netI 0.0869 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 83277 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.275 _diffrn_reflns_theta_min 2.351 _diffrn_ambient_temperature 291.0 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'graphite' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 9757 _reflns_number_total 20924 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.428 _refine_diff_density_min -0.459 _refine_diff_density_rms 0.136 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1132 _refine_ls_number_reflns 20924 _refine_ls_number_restraints 105 _refine_ls_R_factor_all 0.1776 _refine_ls_R_factor_gt 0.0729 _refine_ls_restrained_S_all 1.053 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0799P)^2^+1.3016P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1636 _refine_ls_wR_factor_ref 0.2102 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints O5 \\sim C97 \\sim C98 \\sim C99 \\sim C100: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.01 C18 \\sim C19 \\sim C20 \\sim H20 \\sim C21 \\sim C22 \\sim H22 \\sim C23 \\sim C24 \\sim H24A \\sim H24B \\sim H24C \\sim H97A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 3.a Secondary CH2 refined with riding coordinates: C98(H98A,H98B), C99(H99A,H99B) 3.b Aromatic/amide H refined with riding coordinates: C1(H1), C6(H6), C7(H7), C8(H8), C9(H9), C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C19(H19), C20(H20), C22(H22), C23(H23), C25(H25), C29(H29), C30(H30), C31(H31), C32(H32), C35(H35), C36(H36), C37(H37), C38(H38), C39(H39), C43(H43), C44(H44), C46(H46), C47(H47), C49(H49), C54(H54), C55(H55), C56(H56), C57(H57), C59(H59), C60(H60), C61(H61), C62(H62), C63(H63), C67(H67), C68(H68), C70(H70), C71(H71), C73(H73), C78(H78), C79(H79), C80(H80), C81(H81), C83(H83), C84(H84), C85(H85), C86(H86), C87(H87), C91(H91), C92(H92), C94(H94), C95(H95) 3.c Idealised Me refined as rotating group: C24(H24A,H24B,H24C), C48(H48A,H48B,H48C), C72(H72A,H72B,H72C), C96(H96A,H96B, H96C), C97(H97A,H97B,H97C), C100(H10A,H10B,H10C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F1 F 0.78255(18) 1.10578(11) 0.75786(9) 0.0765(6) Uani 1 1 d . . . . . F2 F 0.76814(16) 1.07635(11) 0.66708(8) 0.0730(5) Uani 1 1 d . . . . . F3 F 0.77892(17) 0.99046(10) 0.72318(9) 0.0741(6) Uani 1 1 d . . . . . O1 O 1.01996(17) 1.05664(10) 0.78030(8) 0.0444(5) Uani 1 1 d . . . . . N1 N 1.2049(2) 1.15365(12) 0.78579(9) 0.0404(5) Uani 1 1 d . . . . . N2 N 1.0136(2) 1.15976(12) 0.72168(9) 0.0454(6) Uani 1 1 d . . . . . C1 C 1.1261(3) 1.19131(15) 0.75093(12) 0.0441(7) Uani 1 1 d . . . . . H1 H 1.1568 1.2425 0.7487 0.053 Uiso 1 1 calc R . . . . C2 C 1.1486(3) 1.08579(14) 0.80328(11) 0.0373(6) Uani 1 1 d . . . . . C3 C 1.2342(2) 1.06289(15) 0.84470(11) 0.0383(6) Uani 1 1 d . . . . . C4 C 1.3539(2) 1.12168(15) 0.85522(11) 0.0408(6) Uani 1 1 d . . . . . C5 C 1.3335(3) 1.17712(15) 0.81841(11) 0.0424(6) Uani 1 1 d . . . . . C6 C 1.4288(3) 1.23999(17) 0.81633(13) 0.0552(8) Uani 1 1 d . . . . . H6 H 1.4129 1.2751 0.7910 0.066 Uiso 1 1 calc R . . . . C7 C 1.5486(3) 1.24828(19) 0.85369(16) 0.0682(10) Uani 1 1 d . . . . . H7 H 1.6154 1.2898 0.8535 0.082 Uiso 1 1 calc R . . . . C8 C 1.5711(3) 1.1957(2) 0.89152(15) 0.0686(10) Uani 1 1 d . . . . . H8 H 1.6526 1.2030 0.9164 0.082 Uiso 1 1 calc R . . . . C9 C 1.4757(3) 1.13300(17) 0.89306(13) 0.0536(8) Uani 1 1 d . . . . . H9 H 1.4921 1.0987 0.9189 0.064 Uiso 1 1 calc R . . . . C10 C 1.2088(3) 0.99321(15) 0.87206(11) 0.0419(6) Uani 1 1 d . . . . . C11 C 1.3104(3) 0.95370(18) 0.88972(13) 0.0563(8) Uani 1 1 d . . . . . H11 H 1.3960 0.9707 0.8833 0.068 Uiso 1 1 calc R . . . . C12 C 1.2857(4) 0.88936(19) 0.91680(15) 0.0729(10) Uani 1 1 d . . . . . H12 H 1.3550 0.8639 0.9285 0.087 Uiso 1 1 calc R . . . . C13 C 1.1607(4) 0.86280(19) 0.92661(15) 0.0699(10) Uani 1 1 d . . . . . H13 H 1.1454 0.8203 0.9456 0.084 Uiso 1 1 calc R . . . . C14 C 1.0581(3) 0.89948(18) 0.90818(14) 0.0626(9) Uani 1 1 d . . . . . H14 H 0.9724 0.8808 0.9138 0.075 Uiso 1 1 calc R . . . . C15 C 1.0811(3) 0.96417(16) 0.88132(12) 0.0507(7) Uani 1 1 d . . . . . H15 H 1.0106 0.9886 0.8693 0.061 Uiso 1 1 calc R . . . . C16 C 0.9771(3) 1.07875(15) 0.72389(11) 0.0413(6) Uani 1 1 d . . . . . C17 C 0.8255(3) 1.06218(17) 0.71820(14) 0.0523(8) Uani 1 1 d . . . . . C18 C 1.0241(3) 1.03074(15) 0.67756(12) 0.0442(7) Uani 1 1 d . U . . . C19 C 1.0305(3) 0.95482(17) 0.68242(15) 0.0614(8) Uani 1 1 d . U . . . H19 H 1.0102 0.9341 0.7149 0.074 Uiso 1 1 calc R . . . . C20 C 1.0675(3) 0.9097(2) 0.63820(18) 0.0777(11) Uani 1 1 d . U . . . H20 H 1.0726 0.8590 0.6420 0.093 Uiso 1 1 calc R U . . . C21 C 1.0968(3) 0.9383(2) 0.58921(17) 0.0761(10) Uani 1 1 d . U . . . C22 C 1.0921(3) 1.0134(2) 0.58547(16) 0.0773(10) Uani 1 1 d . U . . . H22 H 1.1139 1.0341 0.5532 0.093 Uiso 1 1 calc R U . . . C23 C 1.0556(3) 1.05951(19) 0.62864(13) 0.0595(8) Uani 1 1 d . U . . . H23 H 1.0523 1.1104 0.6247 0.071 Uiso 1 1 calc R . . . . C24 C 1.1313(4) 0.8863(3) 0.5416(2) 0.1265(18) Uani 1 1 d . U . . . H24A H 1.1900 0.9158 0.5213 0.190 Uiso 1 1 calc GR U . . . H24B H 1.0512 0.8624 0.5154 0.190 Uiso 1 1 calc GR U . . . H24C H 1.1745 0.8478 0.5577 0.190 Uiso 1 1 calc GR U . . . F4 F 0.76335(17) 0.92974(10) 0.55388(9) 0.0718(5) Uani 1 1 d . . . . . F5 F 0.75055(18) 0.82199(11) 0.50305(9) 0.0821(6) Uani 1 1 d . . . . . F6 F 0.75233(16) 0.82696(11) 0.59322(8) 0.0714(5) Uani 1 1 d . . . . . O2 O 0.51093(16) 0.76603(9) 0.53375(7) 0.0389(4) Uani 1 1 d . . . . . N3 N 0.3298(2) 0.78020(11) 0.46574(9) 0.0362(5) Uani 1 1 d . . . . . N4 N 0.5157(2) 0.87725(12) 0.48293(10) 0.0452(6) Uani 1 1 d . . . . . C25 C 0.4063(3) 0.84343(14) 0.45216(11) 0.0415(6) Uani 1 1 d . . . . . H25 H 0.3762 0.8625 0.4185 0.050 Uiso 1 1 calc R . . . . C26 C 0.3804(2) 0.74294(13) 0.51021(10) 0.0326(6) Uani 1 1 d . . . . . C27 C 0.2887(2) 0.68448(13) 0.51972(10) 0.0320(6) Uani 1 1 d . . . . . C28 C 0.1709(2) 0.68311(13) 0.47631(10) 0.0345(6) Uani 1 1 d . . . . . C29 C 0.0463(2) 0.63536(15) 0.46096(12) 0.0429(6) Uani 1 1 d . . . . . H29 H 0.0248 0.5942 0.4806 0.052 Uiso 1 1 calc R . . . . C30 C -0.0441(3) 0.65025(17) 0.41624(13) 0.0537(8) Uani 1 1 d . . . . . H30 H -0.1275 0.6190 0.4062 0.064 Uiso 1 1 calc R . . . . C31 C -0.0138(3) 0.71064(17) 0.38579(12) 0.0525(8) Uani 1 1 d . . . . . H31 H -0.0773 0.7193 0.3559 0.063 Uiso 1 1 calc R . . . . C32 C 0.1080(3) 0.75783(16) 0.39891(11) 0.0443(7) Uani 1 1 d . . . . . H32 H 0.1286 0.7984 0.3786 0.053 Uiso 1 1 calc R . . . . C33 C 0.1987(2) 0.74280(13) 0.44338(10) 0.0347(6) Uani 1 1 d . . . . . C34 C 0.3066(2) 0.63466(13) 0.56483(10) 0.0338(6) Uani 1 1 d . . . . . C35 C 0.4305(3) 0.61682(15) 0.58446(12) 0.0432(7) Uani 1 1 d . . . . . H35 H 0.5038 0.6366 0.5690 0.052 Uiso 1 1 calc R . . . . C36 C 0.4460(3) 0.56986(17) 0.62680(13) 0.0546(8) Uani 1 1 d . . . . . H36 H 0.5297 0.5590 0.6400 0.066 Uiso 1 1 calc R . . . . C37 C 0.3382(3) 0.53913(18) 0.64955(14) 0.0626(9) Uani 1 1 d . . . . . H37 H 0.3490 0.5070 0.6776 0.075 Uiso 1 1 calc R . . . . C38 C 0.2143(3) 0.55608(18) 0.63077(14) 0.0626(9) Uani 1 1 d . . . . . H38 H 0.1412 0.5353 0.6460 0.075 Uiso 1 1 calc R . . . . C39 C 0.1992(3) 0.60406(16) 0.58924(12) 0.0497(7) Uani 1 1 d . . . . . H39 H 0.1158 0.6162 0.5773 0.060 Uiso 1 1 calc R . . . . C40 C 0.5541(2) 0.84813(14) 0.53631(11) 0.0384(6) Uani 1 1 d . . . . . C41 C 0.7069(3) 0.85669(17) 0.54673(14) 0.0537(8) Uani 1 1 d . . . . . C42 C 0.5089(2) 0.89021(14) 0.58641(11) 0.0383(6) Uani 1 1 d . . . . . C43 C 0.4867(3) 0.96396(15) 0.58528(13) 0.0507(7) Uani 1 1 d . . . . . H43 H 0.4966 0.9878 0.5529 0.061 Uiso 1 1 calc R . . . . C44 C 0.4501(3) 1.00257(18) 0.63160(15) 0.0612(9) Uani 1 1 d . . . . . H44 H 0.4349 1.0522 0.6298 0.073 Uiso 1 1 calc R . . . . C45 C 0.4353(3) 0.9697(2) 0.68054(14) 0.0633(9) Uani 1 1 d . . . . . C46 C 0.4548(3) 0.8952(2) 0.68087(14) 0.0660(9) Uani 1 1 d . . . . . H46 H 0.4425 0.8710 0.7129 0.079 Uiso 1 1 calc R . . . . C47 C 0.4922(3) 0.85549(17) 0.63464(12) 0.0531(8) Uani 1 1 d . . . . . H47 H 0.5060 0.8056 0.6361 0.064 Uiso 1 1 calc R . . . . C48 C 0.3994(4) 1.0134(3) 0.73238(16) 0.1016(14) Uani 1 1 d . . . . . H48A H 0.4789 1.0433 0.7558 0.152 Uiso 1 1 calc GR . . . . H48B H 0.3571 0.9780 0.7544 0.152 Uiso 1 1 calc GR . . . . H48C H 0.3396 1.0466 0.7197 0.152 Uiso 1 1 calc GR . . . . F7 F -0.21209(17) 0.59654(11) 0.26171(8) 0.0702(5) Uani 1 1 d . . . . . F8 F -0.22677(15) 0.56672(10) 0.17090(7) 0.0653(5) Uani 1 1 d . . . . . F9 F -0.20925(16) 0.48160(10) 0.22748(8) 0.0646(5) Uani 1 1 d . . . . . O3 O 0.03053(17) 0.55120(10) 0.28404(7) 0.0405(4) Uani 1 1 d . . . . . N5 N 0.2103(2) 0.65096(12) 0.28878(9) 0.0379(5) Uani 1 1 d . . . . . N6 N 0.0158(2) 0.65453(12) 0.22553(9) 0.0423(5) Uani 1 1 d . . . . . C49 C 0.1285(3) 0.68763(14) 0.25435(11) 0.0403(6) Uani 1 1 d . . . . . H49 H 0.1568 0.7390 0.2520 0.048 Uiso 1 1 calc R . . . . C50 C 0.1582(2) 0.58289(14) 0.30712(10) 0.0348(6) Uani 1 1 d . . . . . C51 C 0.2449(2) 0.56380(14) 0.34984(11) 0.0379(6) Uani 1 1 d . . . . . C52 C 0.3619(3) 0.62387(15) 0.35916(11) 0.0409(6) Uani 1 1 d . . . . . C53 C 0.3377(2) 0.67787(15) 0.32132(11) 0.0400(6) Uani 1 1 d . . . . . C54 C 0.4306(3) 0.74070(16) 0.31718(13) 0.0524(7) Uani 1 1 d . . . . . H54 H 0.4115 0.7750 0.2916 0.063 Uiso 1 1 calc R . . . . C55 C 0.5534(3) 0.75034(19) 0.35273(15) 0.0655(9) Uani 1 1 d . . . . . H55 H 0.6183 0.7923 0.3515 0.079 Uiso 1 1 calc R . . . . C56 C 0.5811(3) 0.6982(2) 0.39022(15) 0.0678(10) Uani 1 1 d . . . . . H56 H 0.6647 0.7059 0.4136 0.081 Uiso 1 1 calc R . . . . C57 C 0.4881(3) 0.63537(17) 0.39371(13) 0.0538(8) Uani 1 1 d . . . . . H57 H 0.5090 0.6008 0.4189 0.065 Uiso 1 1 calc R . . . . C58 C 0.2246(3) 0.49701(15) 0.38121(11) 0.0384(6) Uani 1 1 d . . . . . C59 C 0.2757(3) 0.50398(17) 0.44011(12) 0.0543(8) Uani 1 1 d . . . . . H59 H 0.3210 0.5511 0.4594 0.065 Uiso 1 1 calc R . . . . C60 C 0.2600(3) 0.44212(19) 0.47005(13) 0.0639(9) Uani 1 1 d . . . . . H60 H 0.2941 0.4479 0.5092 0.077 Uiso 1 1 calc R . . . . C61 C 0.1937(3) 0.37159(19) 0.44190(15) 0.0632(9) Uani 1 1 d . . . . . H61 H 0.1836 0.3296 0.4618 0.076 Uiso 1 1 calc R . . . . C62 C 0.1432(3) 0.36417(18) 0.38452(14) 0.0626(9) Uani 1 1 d . . . . . H62 H 0.0983 0.3168 0.3655 0.075 Uiso 1 1 calc R . . . . C63 C 0.1577(3) 0.42585(16) 0.35433(13) 0.0515(7) Uani 1 1 d . . . . . H63 H 0.1219 0.4195 0.3153 0.062 Uiso 1 1 calc R . . . . C64 C -0.0151(2) 0.57335(14) 0.22777(10) 0.0364(6) Uani 1 1 d . . . . . C65 C -0.1676(3) 0.55385(17) 0.22206(12) 0.0462(7) Uani 1 1 d . . . . . C66 C 0.0317(2) 0.52657(15) 0.18040(11) 0.0393(6) Uani 1 1 d . . . . . C67 C 0.0383(3) 0.45041(16) 0.18352(13) 0.0545(8) Uani 1 1 d . . . . . H67 H 0.0188 0.4284 0.2156 0.065 Uiso 1 1 calc R . . . . C68 C 0.0744(3) 0.40677(19) 0.13833(17) 0.0703(10) Uani 1 1 d . . . . . H68 H 0.0791 0.3558 0.1410 0.084 Uiso 1 1 calc R . . . . C69 C 0.1031(3) 0.4371(2) 0.08983(16) 0.0673(10) Uani 1 1 d . . . . . C70 C 0.0979(3) 0.5126(2) 0.08767(14) 0.0685(9) Uani 1 1 d . . . . . H70 H 0.1186 0.5345 0.0557 0.082 Uiso 1 1 calc R . . . . C71 C 0.0625(3) 0.55773(18) 0.13206(13) 0.0532(7) Uani 1 1 d . . . . . H71 H 0.0595 0.6089 0.1293 0.064 Uiso 1 1 calc R . . . . C72 C 0.1360(4) 0.3875(3) 0.04047(18) 0.1096(16) Uani 1 1 d . . . . . H72A H 0.1810 0.3487 0.0551 0.164 Uiso 1 1 calc GR . . . . H72B H 0.1927 0.4184 0.0203 0.164 Uiso 1 1 calc GR . . . . H72C H 0.0552 0.3639 0.0147 0.164 Uiso 1 1 calc GR . . . . F10 F -0.22033(16) 0.42787(10) 0.05708(9) 0.0713(5) Uani 1 1 d . . . . . F11 F -0.23890(18) 0.31958(12) 0.00565(9) 0.0826(6) Uani 1 1 d . . . . . F12 F -0.23856(16) 0.32437(10) 0.09589(8) 0.0710(5) Uani 1 1 d . . . . . O4 O -0.48204(16) 0.26850(9) 0.03573(7) 0.0399(4) Uani 1 1 d . . . . . N7 N -0.65717(19) 0.28793(11) -0.03354(9) 0.0342(5) Uani 1 1 d . . . . . N8 N -0.4658(2) 0.38062(12) -0.01492(10) 0.0437(5) Uani 1 1 d . . . . . C73 C -0.5765(3) 0.34927(13) -0.04630(11) 0.0378(6) Uani 1 1 d . . . . . H73 H -0.6039 0.3694 -0.0798 0.045 Uiso 1 1 calc R . . . . C74 C -0.6113(2) 0.24719(13) 0.01010(10) 0.0326(6) Uani 1 1 d . . . . . C75 C -0.7044(2) 0.18678(13) 0.01456(10) 0.0323(6) Uani 1 1 d . . . . . C76 C -0.8183(2) 0.18839(13) -0.02991(10) 0.0320(5) Uani 1 1 d . . . . . C77 C -0.7867(2) 0.25132(13) -0.05917(10) 0.0326(6) Uani 1 1 d . . . . . C78 C -0.8744(3) 0.27092(14) -0.10282(11) 0.0407(6) Uani 1 1 d . . . . . H78 H -0.8516 0.3136 -0.1208 0.049 Uiso 1 1 calc R . . . . C79 C -0.9973(3) 0.22426(16) -0.11853(12) 0.0488(7) Uani 1 1 d . . . . . H79 H -1.0584 0.2349 -0.1485 0.059 Uiso 1 1 calc R . . . . C80 C -1.0318(3) 0.16196(16) -0.09071(12) 0.0493(7) Uani 1 1 d . . . . . H80 H -1.1160 0.1319 -0.1021 0.059 Uiso 1 1 calc R . . . . C81 C -0.9442(2) 0.14326(14) -0.04646(11) 0.0409(6) Uani 1 1 d . . . . . H81 H -0.9690 0.1013 -0.0281 0.049 Uiso 1 1 calc R . . . . C82 C -0.6944(2) 0.12934(14) 0.05458(11) 0.0346(6) Uani 1 1 d . . . . . C83 C -0.6586(3) 0.15057(17) 0.11337(12) 0.0530(8) Uani 1 1 d . . . . . H83 H -0.6384 0.2021 0.1282 0.064 Uiso 1 1 calc R . . . . C84 C -0.6527(3) 0.0955(2) 0.15055(14) 0.0665(9) Uani 1 1 d . . . . . H84 H -0.6286 0.1106 0.1900 0.080 Uiso 1 1 calc R . . . . C85 C -0.6817(3) 0.02015(19) 0.12953(15) 0.0615(9) Uani 1 1 d . . . . . H85 H -0.6778 -0.0165 0.1545 0.074 Uiso 1 1 calc R . . . . C86 C -0.7171(3) -0.00195(16) 0.07114(14) 0.0547(8) Uani 1 1 d . . . . . H86 H -0.7368 -0.0536 0.0567 0.066 Uiso 1 1 calc R . . . . C87 C -0.7234(3) 0.05210(14) 0.03408(12) 0.0461(7) Uani 1 1 d . . . . . H87 H -0.7476 0.0365 -0.0053 0.055 Uiso 1 1 calc R . . . . C88 C -0.4329(2) 0.35031(14) 0.03857(11) 0.0389(6) Uani 1 1 d . . . . . C89 C -0.2805(3) 0.35553(17) 0.04947(15) 0.0541(8) Uani 1 1 d . . . . . C90 C -0.4776(2) 0.39404(14) 0.08830(11) 0.0367(6) Uani 1 1 d . . . . . C91 C -0.4787(3) 0.36448(16) 0.13978(12) 0.0487(7) Uani 1 1 d . . . . . H91 H -0.4530 0.3176 0.1439 0.058 Uiso 1 1 calc R . . . . C92 C -0.5182(3) 0.40483(18) 0.18534(13) 0.0574(8) Uani 1 1 d . . . . . H92 H -0.5198 0.3840 0.2195 0.069 Uiso 1 1 calc R . . . . C93 C -0.5549(3) 0.47505(18) 0.18110(13) 0.0520(7) Uani 1 1 d . . . . . C94 C -0.5539(3) 0.50298(16) 0.12934(13) 0.0514(7) Uani 1 1 d . . . . . H94 H -0.5800 0.5498 0.1251 0.062 Uiso 1 1 calc R . . . . C95 C -0.5154(3) 0.46385(15) 0.08373(12) 0.0447(7) Uani 1 1 d . . . . . H95 H -0.5148 0.4847 0.0496 0.054 Uiso 1 1 calc R . . . . C96 C -0.5948(3) 0.5194(2) 0.23107(15) 0.0811(11) Uani 1 1 d . . . . . H96A H -0.5171 0.5512 0.2544 0.122 Uiso 1 1 calc GR . . . . H96B H -0.6361 0.4845 0.2537 0.122 Uiso 1 1 calc GR . . . . H96C H -0.6566 0.5508 0.2169 0.122 Uiso 1 1 calc GR . . . . O5 O 0.9821(5) 0.7438(2) 0.74861(17) 0.1562(15) Uani 1 1 d . U . . . C97 C 1.2067(8) 0.7333(4) 0.7513(3) 0.187(3) Uani 1 1 d . U . A 1 H97A H 1.2100 0.7376 0.7116 0.281 Uiso 1 1 calc GR U . A 1 H97B H 1.1884 0.6803 0.7563 0.281 Uiso 1 1 calc GR . . A 1 H97C H 1.2908 0.7571 0.7745 0.281 Uiso 1 1 calc GR . . A 1 C98 C 1.1072(9) 0.7692(4) 0.7677(3) 0.184(3) Uani 1 1 d . U . A 1 H98A H 1.1194 0.7729 0.8093 0.220 Uiso 1 1 calc R . . A 1 H98B H 1.1253 0.8210 0.7587 0.220 Uiso 1 1 calc R . . A 1 C99 C 0.8800(8) 0.7755(4) 0.7632(3) 0.168(2) Uani 1 1 d . U . B 2 H99A H 0.8877 0.7778 0.8046 0.202 Uiso 1 1 calc R . . B 2 H99B H 0.8950 0.8279 0.7551 0.202 Uiso 1 1 calc R . . B 2 C100 C 0.7520(8) 0.7452(4) 0.7400(3) 0.199(3) Uani 1 1 d . U . B 2 H10A H 0.7485 0.7159 0.7035 0.299 Uiso 1 1 calc GR . . B 2 H10B H 0.7018 0.7855 0.7350 0.299 Uiso 1 1 calc GR . . B 2 H10C H 0.7147 0.7126 0.7652 0.299 Uiso 1 1 calc GR . . B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F1 0.0571(11) 0.0938(14) 0.0844(15) 0.0065(12) 0.0212(10) 0.0259(11) F2 0.0473(10) 0.0975(14) 0.0690(13) 0.0237(11) -0.0130(9) 0.0130(10) F3 0.0467(10) 0.0689(12) 0.0999(16) 0.0223(11) -0.0006(10) -0.0031(9) O1 0.0376(10) 0.0519(11) 0.0401(11) 0.0097(9) -0.0025(8) 0.0043(9) N1 0.0394(12) 0.0442(13) 0.0351(13) 0.0023(10) 0.0023(10) 0.0062(10) N2 0.0508(14) 0.0423(13) 0.0415(14) 0.0078(11) -0.0006(11) 0.0112(11) C1 0.0523(17) 0.0377(15) 0.0434(17) 0.0070(13) 0.0059(14) 0.0127(14) C2 0.0393(15) 0.0409(15) 0.0321(15) 0.0025(12) 0.0065(12) 0.0097(12) C3 0.0376(14) 0.0485(16) 0.0305(15) -0.0002(12) 0.0087(12) 0.0138(13) C4 0.0364(15) 0.0506(16) 0.0344(15) -0.0077(12) 0.0063(12) 0.0134(13) C5 0.0392(15) 0.0475(16) 0.0395(16) -0.0052(13) 0.0087(13) 0.0101(13) C6 0.0510(18) 0.0514(18) 0.061(2) -0.0046(15) 0.0158(16) 0.0037(15) C7 0.0435(19) 0.064(2) 0.086(3) -0.0194(19) 0.0086(18) -0.0025(16) C8 0.0404(18) 0.077(2) 0.075(3) -0.023(2) -0.0088(16) 0.0120(18) C9 0.0449(17) 0.062(2) 0.0507(19) -0.0068(15) 0.0001(14) 0.0175(16) C10 0.0458(16) 0.0493(16) 0.0326(15) 0.0015(12) 0.0074(12) 0.0166(13) C11 0.0537(18) 0.068(2) 0.0511(19) 0.0081(16) 0.0075(15) 0.0248(16) C12 0.090(3) 0.067(2) 0.071(2) 0.0192(19) 0.009(2) 0.039(2) C13 0.084(3) 0.058(2) 0.075(3) 0.0233(18) 0.022(2) 0.0177(19) C14 0.065(2) 0.060(2) 0.068(2) 0.0145(17) 0.0217(18) 0.0107(17) C15 0.0515(18) 0.0546(18) 0.0463(18) 0.0049(14) 0.0058(14) 0.0147(15) C16 0.0425(15) 0.0424(15) 0.0364(16) 0.0087(12) -0.0032(12) 0.0077(12) C17 0.0460(17) 0.0538(19) 0.057(2) 0.0126(16) 0.0001(15) 0.0129(15) C18 0.0364(14) 0.0473(16) 0.0437(17) -0.0006(13) -0.0052(12) 0.0086(12) C19 0.0595(19) 0.0528(18) 0.065(2) -0.0045(16) -0.0006(16) 0.0099(15) C20 0.062(2) 0.062(2) 0.097(3) -0.022(2) -0.011(2) 0.0219(17) C21 0.0471(18) 0.099(3) 0.071(2) -0.030(2) -0.0040(17) 0.0211(19) C22 0.063(2) 0.104(3) 0.060(2) -0.009(2) 0.0083(17) 0.019(2) C23 0.0557(18) 0.070(2) 0.050(2) -0.0003(16) 0.0042(15) 0.0143(16) C24 0.083(3) 0.159(4) 0.121(4) -0.072(3) 0.008(3) 0.041(3) F4 0.0501(10) 0.0568(11) 0.0969(15) 0.0009(10) 0.0111(10) -0.0167(9) F5 0.0552(11) 0.0936(15) 0.0946(16) -0.0162(12) 0.0311(11) 0.0058(10) F6 0.0426(10) 0.0821(13) 0.0839(14) 0.0185(11) -0.0053(9) 0.0064(9) O2 0.0355(10) 0.0317(9) 0.0459(11) 0.0051(8) 0.0021(8) 0.0009(8) N3 0.0404(12) 0.0331(11) 0.0343(12) 0.0070(9) 0.0047(10) 0.0043(10) N4 0.0539(15) 0.0388(12) 0.0392(14) 0.0063(10) 0.0068(11) -0.0022(11) C25 0.0548(17) 0.0360(15) 0.0343(15) 0.0079(12) 0.0090(13) 0.0068(13) C26 0.0355(14) 0.0281(13) 0.0328(14) 0.0014(11) 0.0035(11) 0.0064(11) C27 0.0343(13) 0.0306(13) 0.0321(14) 0.0042(11) 0.0065(11) 0.0078(11) C28 0.0358(14) 0.0358(14) 0.0330(14) 0.0027(11) 0.0068(11) 0.0101(11) C29 0.0358(14) 0.0460(16) 0.0448(17) 0.0065(13) 0.0048(12) 0.0033(12) C30 0.0357(15) 0.0616(19) 0.057(2) 0.0033(16) -0.0022(14) 0.0019(14) C31 0.0471(17) 0.064(2) 0.0423(18) 0.0088(15) -0.0063(14) 0.0119(15) C32 0.0494(17) 0.0508(17) 0.0328(15) 0.0088(13) 0.0023(13) 0.0125(14) C33 0.0367(14) 0.0358(14) 0.0313(14) 0.0018(11) 0.0058(11) 0.0080(11) C34 0.0379(14) 0.0288(13) 0.0339(15) 0.0032(11) 0.0058(11) 0.0049(11) C35 0.0372(15) 0.0480(16) 0.0468(17) 0.0108(13) 0.0105(13) 0.0090(13) C36 0.0483(17) 0.0632(19) 0.059(2) 0.0238(16) 0.0071(15) 0.0216(15) C37 0.066(2) 0.068(2) 0.063(2) 0.0376(18) 0.0157(17) 0.0156(17) C38 0.0546(19) 0.078(2) 0.061(2) 0.0327(18) 0.0192(16) 0.0070(17) C39 0.0404(16) 0.0632(19) 0.0499(18) 0.0180(15) 0.0112(14) 0.0120(14) C40 0.0394(15) 0.0329(14) 0.0405(16) 0.0040(12) 0.0080(12) -0.0009(12) C41 0.0466(17) 0.0468(18) 0.064(2) 0.0005(16) 0.0128(16) -0.0011(15) C42 0.0340(14) 0.0386(15) 0.0374(16) -0.0010(12) 0.0022(12) 0.0000(12) C43 0.0546(18) 0.0400(16) 0.0541(19) 0.0014(14) 0.0088(15) 0.0020(14) C44 0.0554(19) 0.0527(19) 0.070(2) -0.0125(17) 0.0085(17) 0.0110(15) C45 0.0409(17) 0.087(3) 0.053(2) -0.0211(18) 0.0033(15) 0.0103(17) C46 0.064(2) 0.094(3) 0.0390(19) 0.0098(18) 0.0090(16) 0.0119(19) C47 0.0613(19) 0.0566(18) 0.0421(18) 0.0103(15) 0.0064(15) 0.0131(15) C48 0.078(3) 0.143(4) 0.077(3) -0.038(3) 0.014(2) 0.034(3) F7 0.0531(11) 0.0899(14) 0.0721(13) 0.0042(11) 0.0212(9) 0.0201(10) F8 0.0399(9) 0.0939(14) 0.0571(11) 0.0249(10) -0.0101(8) 0.0062(9) F9 0.0464(10) 0.0659(11) 0.0757(13) 0.0199(10) 0.0041(9) -0.0071(9) O3 0.0391(10) 0.0459(10) 0.0329(10) 0.0089(8) -0.0019(8) 0.0030(8) N5 0.0363(12) 0.0414(12) 0.0329(12) 0.0021(10) 0.0006(10) 0.0057(10) N6 0.0430(13) 0.0423(13) 0.0397(13) 0.0078(10) 0.0006(11) 0.0077(11) C49 0.0460(16) 0.0354(14) 0.0387(16) 0.0058(12) 0.0051(13) 0.0069(13) C50 0.0356(14) 0.0399(15) 0.0277(14) 0.0004(11) 0.0044(11) 0.0075(12) C51 0.0390(14) 0.0437(15) 0.0297(14) -0.0051(12) 0.0004(11) 0.0159(12) C52 0.0379(15) 0.0466(16) 0.0355(15) -0.0093(12) 0.0019(12) 0.0136(13) C53 0.0356(14) 0.0452(16) 0.0368(16) -0.0079(12) 0.0058(12) 0.0091(13) C54 0.0475(17) 0.0515(18) 0.0539(19) -0.0067(14) 0.0130(15) 0.0008(15) C55 0.0435(18) 0.068(2) 0.074(2) -0.0168(19) 0.0068(17) -0.0026(16) C56 0.0393(17) 0.082(2) 0.069(2) -0.0214(19) -0.0109(16) 0.0130(18) C57 0.0453(17) 0.060(2) 0.0500(19) -0.0087(15) -0.0067(14) 0.0179(16) C58 0.0417(15) 0.0443(15) 0.0319(15) -0.0001(12) 0.0050(12) 0.0210(13) C59 0.072(2) 0.0561(18) 0.0362(17) -0.0021(14) 0.0024(15) 0.0284(16) C60 0.089(2) 0.072(2) 0.0395(18) 0.0140(17) 0.0100(17) 0.038(2) C61 0.076(2) 0.066(2) 0.061(2) 0.0242(18) 0.0226(19) 0.0309(19) C62 0.072(2) 0.0540(19) 0.062(2) 0.0092(17) 0.0095(18) 0.0122(17) C63 0.0539(18) 0.0559(19) 0.0413(17) 0.0030(14) 0.0000(14) 0.0107(15) C64 0.0361(14) 0.0401(15) 0.0300(14) 0.0082(11) -0.0030(11) 0.0049(12) C65 0.0407(16) 0.0541(18) 0.0439(18) 0.0131(14) 0.0038(13) 0.0080(14) C66 0.0311(13) 0.0472(16) 0.0346(15) 0.0010(12) -0.0044(11) 0.0054(12) C67 0.0561(18) 0.0475(18) 0.053(2) -0.0017(15) -0.0050(15) 0.0088(15) C68 0.059(2) 0.055(2) 0.083(3) -0.0206(19) -0.0148(19) 0.0179(17) C69 0.0418(18) 0.089(3) 0.062(2) -0.023(2) -0.0017(16) 0.0148(18) C70 0.055(2) 0.101(3) 0.049(2) -0.0016(19) 0.0137(16) 0.015(2) C71 0.0472(17) 0.0634(19) 0.0471(19) 0.0033(15) 0.0062(14) 0.0094(15) C72 0.074(3) 0.142(4) 0.100(3) -0.051(3) 0.014(2) 0.030(3) F10 0.0440(10) 0.0575(11) 0.0994(15) 0.0018(10) 0.0036(9) -0.0148(9) F11 0.0518(11) 0.0960(15) 0.0958(16) -0.0180(12) 0.0240(11) 0.0104(10) F12 0.0454(10) 0.0749(12) 0.0865(14) 0.0167(11) -0.0101(9) 0.0103(9) O4 0.0363(10) 0.0305(9) 0.0481(11) 0.0049(8) -0.0021(8) 0.0021(8) N7 0.0360(11) 0.0283(11) 0.0367(12) 0.0067(9) 0.0043(9) 0.0017(9) N8 0.0480(14) 0.0359(12) 0.0426(14) 0.0060(10) 0.0069(11) -0.0051(11) C73 0.0452(15) 0.0322(14) 0.0346(15) 0.0059(11) 0.0072(12) 0.0018(12) C74 0.0342(13) 0.0291(13) 0.0337(14) 0.0049(11) 0.0030(11) 0.0058(11) C75 0.0357(13) 0.0301(13) 0.0308(14) 0.0026(10) 0.0067(11) 0.0055(11) C76 0.0357(14) 0.0311(13) 0.0281(14) 0.0010(10) 0.0063(11) 0.0044(11) C77 0.0339(13) 0.0300(13) 0.0319(14) 0.0015(11) 0.0040(11) 0.0036(11) C78 0.0474(16) 0.0376(14) 0.0358(16) 0.0091(12) 0.0041(13) 0.0048(13) C79 0.0465(17) 0.0582(18) 0.0379(17) 0.0117(14) -0.0049(13) 0.0070(14) C80 0.0390(15) 0.0560(18) 0.0476(18) 0.0083(14) 0.0007(13) -0.0008(13) C81 0.0395(15) 0.0403(15) 0.0402(16) 0.0066(12) 0.0065(12) -0.0013(12) C82 0.0320(13) 0.0372(14) 0.0351(15) 0.0094(11) 0.0069(11) 0.0034(11) C83 0.065(2) 0.0509(17) 0.0381(17) 0.0047(14) 0.0018(15) 0.0048(15) C84 0.082(2) 0.077(2) 0.0376(18) 0.0183(17) -0.0004(16) 0.010(2) C85 0.061(2) 0.062(2) 0.065(2) 0.0346(18) 0.0077(17) 0.0090(17) C86 0.0605(19) 0.0406(16) 0.061(2) 0.0150(15) 0.0068(16) 0.0007(14) C87 0.0559(18) 0.0382(15) 0.0424(17) 0.0070(13) 0.0072(14) 0.0040(13) C88 0.0372(14) 0.0303(13) 0.0441(17) 0.0029(12) 0.0024(12) -0.0032(11) C89 0.0401(16) 0.0493(18) 0.068(2) 0.0020(16) 0.0076(16) -0.0012(14) C90 0.0313(13) 0.0352(14) 0.0381(16) 0.0031(12) -0.0016(11) -0.0019(11) C91 0.0533(17) 0.0437(16) 0.0437(18) 0.0053(13) -0.0046(14) 0.0066(14) C92 0.0577(19) 0.069(2) 0.0403(18) 0.0094(16) 0.0001(15) 0.0045(17) C93 0.0339(15) 0.065(2) 0.051(2) -0.0061(15) 0.0031(13) 0.0049(14) C94 0.0464(17) 0.0464(17) 0.060(2) 0.0005(15) 0.0063(15) 0.0103(14) C95 0.0451(16) 0.0391(15) 0.0471(18) 0.0061(13) 0.0046(13) 0.0028(13) C96 0.067(2) 0.113(3) 0.062(2) -0.017(2) 0.0125(18) 0.030(2) O5 0.150(4) 0.167(4) 0.134(3) -0.024(3) 0.009(3) 0.019(3) C97 0.178(7) 0.184(6) 0.200(7) 0.027(5) 0.021(5) 0.044(5) C98 0.176(6) 0.168(5) 0.185(6) 0.012(5) -0.016(5) 0.021(5) C99 0.173(6) 0.152(5) 0.162(5) -0.028(4) 0.013(5) 0.023(5) C100 0.185(7) 0.216(7) 0.187(6) -0.050(5) 0.055(6) 0.036(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F1 C17 1.336(3) . ? F2 C17 1.333(3) . ? F3 C17 1.321(3) . ? O1 C2 1.350(3) . ? O1 C16 1.460(3) . ? N1 C1 1.371(3) . ? N1 C2 1.394(3) . ? N1 C5 1.403(3) . ? N2 C1 1.267(3) . ? N2 C16 1.447(3) . ? C2 C3 1.358(3) . ? C3 C4 1.459(4) . ? C3 C10 1.472(4) . ? C4 C5 1.409(4) . ? C4 C9 1.398(4) . ? C5 C6 1.382(4) . ? C6 C7 1.381(4) . ? C7 C8 1.389(5) . ? C8 C9 1.377(4) . ? C10 C11 1.392(4) . ? C10 C15 1.399(4) . ? C11 C12 1.385(4) . ? C12 C13 1.368(5) . ? C13 C14 1.372(4) . ? C14 C15 1.386(4) . ? C16 C17 1.527(4) . ? C16 C18 1.514(4) . ? C18 C19 1.386(4) . ? C18 C23 1.385(4) . ? C19 C20 1.398(5) . ? C20 C21 1.378(5) . ? C21 C22 1.364(5) . ? C21 C24 1.512(5) . ? C22 C23 1.387(4) . ? F4 C41 1.325(3) . ? F5 C41 1.331(3) . ? F6 C41 1.328(3) . ? O2 C26 1.355(3) . ? O2 C40 1.457(3) . ? N3 C25 1.371(3) . ? N3 C26 1.385(3) . ? N3 C33 1.404(3) . ? N4 C25 1.267(3) . ? N4 C40 1.444(3) . ? C26 C27 1.358(3) . ? C27 C28 1.460(3) . ? C27 C34 1.473(3) . ? C28 C29 1.398(3) . ? C28 C33 1.409(3) . ? C29 C30 1.377(4) . ? C30 C31 1.385(4) . ? C31 C32 1.369(4) . ? C32 C33 1.376(3) . ? C34 C35 1.389(3) . ? C34 C39 1.395(3) . ? C35 C36 1.384(3) . ? C36 C37 1.376(4) . ? C37 C38 1.379(4) . ? C38 C39 1.382(4) . ? C40 C41 1.538(4) . ? C40 C42 1.519(4) . ? C42 C43 1.377(3) . ? C42 C47 1.382(4) . ? C43 C44 1.375(4) . ? C44 C45 1.377(4) . ? C45 C46 1.380(4) . ? C45 C48 1.518(4) . ? C46 C47 1.386(4) . ? F7 C65 1.335(3) . ? F8 C65 1.332(3) . ? F9 C65 1.322(3) . ? O3 C50 1.352(3) . ? O3 C64 1.463(3) . ? N5 C49 1.373(3) . ? N5 C50 1.393(3) . ? N5 C53 1.399(3) . ? N6 C49 1.271(3) . ? N6 C64 1.445(3) . ? C50 C51 1.354(3) . ? C51 C52 1.454(4) . ? C51 C58 1.478(4) . ? C52 C53 1.412(4) . ? C52 C57 1.398(4) . ? C53 C54 1.379(4) . ? C54 C55 1.383(4) . ? C55 C56 1.388(4) . ? C56 C57 1.377(4) . ? C58 C59 1.401(4) . ? C58 C63 1.383(4) . ? C59 C60 1.379(4) . ? C60 C61 1.382(4) . ? C61 C62 1.366(4) . ? C62 C63 1.380(4) . ? C64 C65 1.538(4) . ? C64 C66 1.519(4) . ? C66 C67 1.384(4) . ? C66 C71 1.389(4) . ? C67 C68 1.395(4) . ? C68 C69 1.379(5) . ? C69 C70 1.368(5) . ? C69 C72 1.512(5) . ? C70 C71 1.392(4) . ? F10 C89 1.324(3) . ? F11 C89 1.333(3) . ? F12 C89 1.331(3) . ? O4 C74 1.353(3) . ? O4 C88 1.461(3) . ? N7 C73 1.360(3) . ? N7 C74 1.395(3) . ? N7 C77 1.403(3) . ? N8 C73 1.271(3) . ? N8 C88 1.447(3) . ? C74 C75 1.352(3) . ? C75 C76 1.457(3) . ? C75 C82 1.477(3) . ? C76 C77 1.406(3) . ? C76 C81 1.390(3) . ? C77 C78 1.378(3) . ? C78 C79 1.376(4) . ? C79 C80 1.382(4) . ? C80 C81 1.380(4) . ? C82 C83 1.384(4) . ? C82 C87 1.384(3) . ? C83 C84 1.393(4) . ? C84 C85 1.357(4) . ? C85 C86 1.377(4) . ? C86 C87 1.378(3) . ? C88 C89 1.540(4) . ? C88 C90 1.523(4) . ? C90 C91 1.385(4) . ? C90 C95 1.376(3) . ? C91 C92 1.390(4) . ? C92 C93 1.378(4) . ? C93 C94 1.377(4) . ? C93 C96 1.508(4) . ? C94 C95 1.375(4) . ? O5 C98 1.290(8) . ? O5 C99 1.350(7) . ? C97 C98 1.380(8) . ? C99 C100 1.349(8) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O1 C16 113.58(19) . . ? C1 N1 C2 119.6(2) . . ? C1 N1 C5 131.4(2) . . ? C2 N1 C5 107.8(2) . . ? C1 N2 C16 115.3(2) . . ? N2 C1 N1 123.2(2) . . ? O1 C2 N1 117.3(2) . . ? O1 C2 C3 130.8(2) . . ? C3 C2 N1 111.8(2) . . ? C2 C3 C4 105.0(2) . . ? C2 C3 C10 126.4(2) . . ? C4 C3 C10 128.6(2) . . ? C5 C4 C3 108.6(2) . . ? C9 C4 C3 133.8(3) . . ? C9 C4 C5 117.7(3) . . ? N1 C5 C4 106.8(2) . . ? C6 C5 N1 129.6(3) . . ? C6 C5 C4 123.6(3) . . ? C7 C6 C5 116.8(3) . . ? C6 C7 C8 121.1(3) . . ? C9 C8 C7 121.6(3) . . ? C8 C9 C4 119.2(3) . . ? C11 C10 C3 121.5(3) . . ? C11 C10 C15 117.4(3) . . ? C15 C10 C3 121.1(2) . . ? C12 C11 C10 120.8(3) . . ? C13 C12 C11 120.9(3) . . ? C12 C13 C14 119.4(3) . . ? C13 C14 C15 120.5(3) . . ? C14 C15 C10 120.9(3) . . ? O1 C16 C17 101.8(2) . . ? O1 C16 C18 110.7(2) . . ? N2 C16 O1 113.4(2) . . ? N2 C16 C17 106.3(2) . . ? N2 C16 C18 112.3(2) . . ? C18 C16 C17 111.8(2) . . ? F1 C17 C16 112.4(3) . . ? F2 C17 F1 106.8(2) . . ? F2 C17 C16 110.2(2) . . ? F3 C17 F1 106.7(3) . . ? F3 C17 F2 107.7(2) . . ? F3 C17 C16 112.7(2) . . ? C19 C18 C16 119.7(3) . . ? C23 C18 C16 121.8(2) . . ? C23 C18 C19 118.4(3) . . ? C18 C19 C20 119.6(3) . . ? C21 C20 C19 121.8(3) . . ? C20 C21 C24 119.8(4) . . ? C22 C21 C20 117.9(3) . . ? C22 C21 C24 122.3(4) . . ? C21 C22 C23 121.5(4) . . ? C18 C23 C22 120.8(3) . . ? C26 O2 C40 112.49(17) . . ? C25 N3 C26 119.9(2) . . ? C25 N3 C33 132.0(2) . . ? C26 N3 C33 108.04(19) . . ? C25 N4 C40 116.0(2) . . ? N4 C25 N3 123.6(2) . . ? O2 C26 N3 116.9(2) . . ? O2 C26 C27 131.0(2) . . ? C27 C26 N3 111.9(2) . . ? C26 C27 C28 105.0(2) . . ? C26 C27 C34 126.5(2) . . ? C28 C27 C34 128.5(2) . . ? C29 C28 C27 134.0(2) . . ? C29 C28 C33 117.5(2) . . ? C33 C28 C27 108.5(2) . . ? C30 C29 C28 119.0(3) . . ? C29 C30 C31 121.6(3) . . ? C32 C31 C30 121.1(3) . . ? C31 C32 C33 117.4(3) . . ? N3 C33 C28 106.6(2) . . ? C32 C33 N3 130.0(2) . . ? C32 C33 C28 123.4(2) . . ? C35 C34 C27 121.2(2) . . ? C35 C34 C39 118.0(2) . . ? C39 C34 C27 120.8(2) . . ? C36 C35 C34 120.7(2) . . ? C37 C36 C35 120.4(3) . . ? C36 C37 C38 119.9(3) . . ? C37 C38 C39 119.7(3) . . ? C38 C39 C34 121.3(3) . . ? O2 C40 C41 102.7(2) . . ? O2 C40 C42 110.0(2) . . ? N4 C40 O2 113.9(2) . . ? N4 C40 C41 106.8(2) . . ? N4 C40 C42 112.3(2) . . ? C42 C40 C41 110.7(2) . . ? F4 C41 F5 107.2(2) . . ? F4 C41 F6 107.8(3) . . ? F4 C41 C40 110.6(2) . . ? F5 C41 C40 112.4(3) . . ? F6 C41 F5 106.7(3) . . ? F6 C41 C40 111.7(2) . . ? C43 C42 C40 120.9(2) . . ? C43 C42 C47 118.8(3) . . ? C47 C42 C40 120.3(2) . . ? C44 C43 C42 120.5(3) . . ? C43 C44 C45 121.7(3) . . ? C44 C45 C46 117.4(3) . . ? C44 C45 C48 121.6(3) . . ? C46 C45 C48 121.0(4) . . ? C45 C46 C47 121.6(3) . . ? C42 C47 C46 119.9(3) . . ? C50 O3 C64 113.65(18) . . ? C49 N5 C50 120.0(2) . . ? C49 N5 C53 130.2(2) . . ? C50 N5 C53 108.2(2) . . ? C49 N6 C64 114.7(2) . . ? N6 C49 N5 123.0(2) . . ? O3 C50 N5 117.1(2) . . ? O3 C50 C51 131.1(2) . . ? C51 C50 N5 111.5(2) . . ? C50 C51 C52 105.3(2) . . ? C50 C51 C58 127.5(2) . . ? C52 C51 C58 127.2(2) . . ? C53 C52 C51 108.6(2) . . ? C57 C52 C51 134.0(3) . . ? C57 C52 C53 117.2(3) . . ? N5 C53 C52 106.4(2) . . ? C54 C53 N5 129.7(3) . . ? C54 C53 C52 123.7(3) . . ? C53 C54 C55 117.0(3) . . ? C54 C55 C56 120.9(3) . . ? C57 C56 C55 121.6(3) . . ? C56 C57 C52 119.5(3) . . ? C59 C58 C51 120.1(2) . . ? C63 C58 C51 122.4(2) . . ? C63 C58 C59 117.5(3) . . ? C60 C59 C58 121.2(3) . . ? C59 C60 C61 120.0(3) . . ? C62 C61 C60 119.3(3) . . ? C61 C62 C63 121.0(3) . . ? C62 C63 C58 121.0(3) . . ? O3 C64 C65 102.06(19) . . ? O3 C64 C66 111.14(19) . . ? N6 C64 O3 113.9(2) . . ? N6 C64 C65 105.9(2) . . ? N6 C64 C66 112.5(2) . . ? C66 C64 C65 110.7(2) . . ? F7 C65 C64 112.0(2) . . ? F8 C65 F7 107.0(2) . . ? F8 C65 C64 110.3(2) . . ? F9 C65 F7 107.1(2) . . ? F9 C65 F8 107.9(2) . . ? F9 C65 C64 112.3(2) . . ? C67 C66 C64 120.1(2) . . ? C67 C66 C71 118.6(3) . . ? C71 C66 C64 121.2(2) . . ? C66 C67 C68 119.7(3) . . ? C69 C68 C67 121.9(3) . . ? C68 C69 C72 120.7(4) . . ? C70 C69 C68 117.7(3) . . ? C70 C69 C72 121.6(4) . . ? C69 C70 C71 121.8(3) . . ? C66 C71 C70 120.2(3) . . ? C74 O4 C88 113.06(17) . . ? C73 N7 C74 120.6(2) . . ? C73 N7 C77 131.4(2) . . ? C74 N7 C77 107.95(18) . . ? C73 N8 C88 115.7(2) . . ? N8 C73 N7 123.6(2) . . ? O4 C74 N7 116.8(2) . . ? C75 C74 O4 131.3(2) . . ? C75 C74 N7 111.4(2) . . ? C74 C75 C76 105.5(2) . . ? C74 C75 C82 128.2(2) . . ? C76 C75 C82 126.3(2) . . ? C77 C76 C75 108.4(2) . . ? C81 C76 C75 133.5(2) . . ? C81 C76 C77 118.1(2) . . ? N7 C77 C76 106.7(2) . . ? C78 C77 N7 129.8(2) . . ? C78 C77 C76 123.5(2) . . ? C79 C78 C77 116.8(2) . . ? C78 C79 C80 121.3(3) . . ? C81 C80 C79 121.6(3) . . ? C80 C81 C76 118.8(2) . . ? C83 C82 C75 121.5(2) . . ? C83 C82 C87 118.0(2) . . ? C87 C82 C75 120.5(2) . . ? C82 C83 C84 120.7(3) . . ? C85 C84 C83 120.3(3) . . ? C84 C85 C86 119.7(3) . . ? C85 C86 C87 120.3(3) . . ? C86 C87 C82 120.9(3) . . ? O4 C88 C89 102.8(2) . . ? O4 C88 C90 109.9(2) . . ? N8 C88 O4 114.3(2) . . ? N8 C88 C89 106.0(2) . . ? N8 C88 C90 112.2(2) . . ? C90 C88 C89 111.2(2) . . ? F10 C89 F11 107.6(3) . . ? F10 C89 F12 108.1(2) . . ? F10 C89 C88 110.2(2) . . ? F11 C89 C88 112.1(3) . . ? F12 C89 F11 106.8(3) . . ? F12 C89 C88 111.8(2) . . ? C91 C90 C88 120.1(2) . . ? C95 C90 C88 121.3(2) . . ? C95 C90 C91 118.5(3) . . ? C90 C91 C92 120.1(3) . . ? C93 C92 C91 121.5(3) . . ? C92 C93 C96 121.4(3) . . ? C94 C93 C92 117.3(3) . . ? C94 C93 C96 121.4(3) . . ? C95 C94 C93 122.0(3) . . ? C94 C95 C90 120.5(3) . . ? O5 C98 C97 123.1(8) . . ? C100 C99 O5 121.7(7) . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 0 0 87.99 3.2 -2 0 0 78.89 3.3 2 0 0 85.99 3.2 2 0 0 82.69 3.3 -3 0 0 1724.43 49.8 -3 0 0 1648.54 49.9 -3 0 0 1668.43 49.99 3 0 0 1633.64 49.8 3 0 0 1611.24 49.7 3 0 0 1704.03 49.99 -4 0 0 6494.25 184.08 -4 0 0 6109.99 184.18 4 0 0 6151.58 183.88 4 0 0 6237.98 184.08 -5 0 0 480.05 16.4 -5 0 0 482.85 16.4 -5 0 0 476.65 16.2 5 0 0 462.45 16.6 5 0 0 496.75 16.4 5 0 0 489.15 16 5 0 0 485.75 16.2 -6 0 0 0.7 2.4 -6 0 0 -1 2.1 6 0 0 2.2 2.5 6 0 0 2.2 2.4 6 0 0 1.5 2.1 6 0 0 3.2 2 -7 0 0 156.48 8 -7 0 0 172.08 8.6 7 0 0 159.88 8.1 7 0 0 164.48 7.7 7 0 0 157.68 7.4 7 0 0 159.88 8.4 -8 0 0 1.6 3.1 -8 0 0 5.9 4.1 8 0 0 8.1 3.2 8 0 0 9.5 3.4 8 0 0 3.6 3.5 -9 0 0 192.08 11.6 -9 0 0 207.18 10.6 9 0 0 205.98 9.7 9 0 0 213.48 10.7 9 0 0 199.18 10.9 -10 0 0 -0.9 4.5 -10 0 0 -7.6 5.5 10 0 0 7.7 4.8 10 0 0 4.3 4.5 10 0 0 6.5 4.2 -11 0 0 46.9 8.9 -11 0 0 47.2 7.3 11 0 0 70.19 8.8 11 0 0 58.79 7.2 11 0 0 58.59 6.9 -12 0 0 4.9 9.3 -12 0 0 0.2 6.4 12 0 0 12 5.7 12 0 0 8 4.8 12 0 0 21.7 8.3 -13 0 0 -9.9 8.3 13 0 0 7.8 5.1 13 0 0 14.6 7.6 13 -1 0 7 6.7 12 -1 0 -4.6 3.9 12 -1 0 0 3.6 -12 1 0 -7 6.1 -12 1 0 6.4 9.5 11 -1 0 -4.1 4.2 11 -1 0 -1.8 3.3 11 -1 0 7.9 5.3 -11 1 0 -1.1 6.9 -11 1 0 -1.4 5 10 -1 0 9.5 5.2 10 -1 0 2.3 3.8 10 -1 0 4.8 3.5 -10 1 0 4.4 5.6 -10 1 0 6.6 4.4 9 -1 0 9.8 3.3 9 -1 0 0 4.3 9 -1 0 0.4 3.4 -9 1 0 3.6 4.7 -9 1 0 7.4 3.7 8 -1 0 18.2 3.9 8 -1 0 19.6 3.9 8 -1 0 20.8 4.6 8 -1 0 19.1 3.5 -8 1 0 22 4 -8 1 0 34 5.2 7 -1 0 -3.5 2 7 -1 0 -1.3 2.4 7 -1 0 -4.2 2.1 7 -1 0 0.3 2.8 -7 1 0 -3.1 2.7 -7 1 0 0.6 2.4 6 -1 0 0.5 2.1 6 -1 0 -1.4 1.9 6 -1 0 1.1 2.4 6 -1 0 0.4 1.9 -6 1 0 -3.2 2.1 -6 1 0 -2.8 1.9 5 -1 0 401.06 14.6 5 -1 0 402.16 14.1 5 -1 0 413.26 13.4 5 -1 0 393.26 13.8 -5 1 0 434.36 14.2 4 -1 0 122.99 5.4 4 -1 0 143.49 5.2 4 -1 0 128.49 6.2 4 -1 0 141.49 5.8 -4 1 0 125.19 5.5 -4 1 0 146.79 5.6 -4 1 0 132.69 5.7 3 -1 0 557.04 18.4 3 -1 0 611.14 18.4 3 -1 0 616.14 18.8 3 -1 0 576.14 19.2 -3 1 0 586.54 18.7 -3 1 0 684.63 18.6 -3 1 0 563.34 18.6 2 -1 0 -0.2 0.4 2 -1 0 -0.7 0.5 2 -1 0 -0.3 0.7 2 -1 0 0.2 0.9 -2 1 0 -0.6 0.8 -2 1 0 -0.1 0.5 -2 1 0 0.4 0.6 -2 -1 0 -1.2 0.9 -2 -1 0 1 0.7 2 1 0 -0.6 0.6 2 1 0 -1 0.8 2 1 0 -0.4 1 -3 -1 0 1160.18 33.6 -3 -1 0 1100.89 33 3 1 0 1020.3 32.9 3 1 0 1014.5 33.4 3 1 0 1171.38 33.4 -4 -1 0 67.49 4.2 -4 -1 0 70.99 3.7 -4 -1 0 68.89 4.3 4 1 0 61.19 4.1 4 1 0 64.39 3.5 4 1 0 75.29 4.1 -5 -1 0 32.6 3.7 -5 -1 0 35.9 3.9 -5 -1 0 33.1 4.2 5 1 0 36.5 4 5 1 0 43 3.9 5 1 0 28.5 3.2 -6 -1 0 1.7 2.2 -6 -1 0 -1.2 2.4 6 1 0 -0.5 2.3 6 1 0 0.3 2.2 6 1 0 -0.1 1.9 -7 -1 0 15.3 3.5 -7 -1 0 12.8 3.6 7 1 0 15.6 3.2 7 1 0 12.6 3.6 7 1 0 16.5 3.7 7 1 0 12.7 3.3 -8 -1 0 -6.5 4.7 -8 -1 0 2.3 3.4 8 1 0 3.3 3.8 8 1 0 2.6 3.3 8 1 0 -5.2 3.4 -9 -1 0 17.6 5.3 -9 -1 0 21.6 5.1 9 1 0 12.4 4.3 9 1 0 17.6 5 9 1 0 19.4 5 -10 -1 0 -3.5 4.6 -10 -1 0 0 6.1 10 1 0 -1.9 4.9 10 1 0 -5.5 4 10 1 0 -0.4 4.6 -11 -1 0 -14.2 5.9 -11 -1 0 3 7.7 11 1 0 -6.5 5.3 11 1 0 -9.3 5.6 11 1 0 0.4 5.3 -12 -1 0 40.8 10.8 -12 -1 0 3.6 7.2 12 1 0 -10.9 6.2 12 1 0 10.2 6.2 12 1 0 8.7 7 -13 -1 0 -2.8 8.5 13 1 0 0.4 6.2 13 1 0 -7.4 6.7 13 -2 0 5 6.8 -13 2 0 2.1 8 12 -2 0 11.2 6.4 -12 2 0 -10.1 6.3 -12 2 0 -3.2 8.1 11 -2 0 0.8 5.4 -11 2 0 -6.1 4.6 -11 2 0 7.9 6.6 10 -2 0 0 2.9 10 -2 0 5.5 4.4 10 -2 0 7.5 2.7 -10 2 0 12.4 5.5 -10 2 0 4.3 4.3 9 -2 0 110.39 6.1 9 -2 0 106.39 8.5 9 -2 0 98.89 5.4 -9 2 0 107.49 7.5 8 -2 0 106.49 6.9 8 -2 0 110.79 5.6 8 -2 0 115.59 6 8 -2 0 113.19 7.9 -8 2 0 117.09 7.6 -8 2 0 104.49 6.7 7 -2 0 1.6 1.8 7 -2 0 2 2.5 7 -2 0 1.6 2.1 7 -2 0 -0.9 2.6 -7 2 0 -2.3 2.5 -7 2 0 6.9 2.6 6 -2 0 170.28 6.5 6 -2 0 179.88 7.9 6 -2 0 178.98 7 6 -2 0 161.38 8.3 -6 2 0 173.78 7.6 5 -2 0 477.25 15.1 5 -2 0 498.55 15.5 5 -2 0 497.85 17 5 -2 0 477.95 16.4 -5 2 0 475.25 15.9 -5 2 0 474.55 15.8 4 -2 0 1000.5 31.4 4 -2 0 1013.9 30 4 -2 0 981 30.9 -4 2 0 1005.1 30.4 -4 2 0 1003.5 30.9 -4 2 0 970.4 30.2 3 -2 0 941.51 28.7 3 -2 0 1004.4 29.1 3 -2 0 804.62 27.5 -3 2 0 912.41 27.9 -3 2 0 1012.5 28.7 -3 2 0 929.11 28.1 2 -2 0 2697.33 80.09 2 -2 0 2589.64 79.79 -2 2 0 2660.43 79.79 -2 2 0 2846.02 80.09 -1 2 0 0.1 0.6 -1 2 0 -0.3 0.4 -1 2 0 -0.7 0.4 -1 -2 0 303.57 10.9 -1 -2 0 359.26 10.9 1 2 0 359.96 11 -2 -2 0 1282.67 36.8 -2 -2 0 1219.48 37.6 -2 -2 0 1225.28 37.5 2 2 0 1234.78 36.7 2 2 0 1226.78 37.6 2 2 0 1251.97 37.6 -3 -2 0 747.03 21.8 -3 -2 0 705.53 22.8 -3 -2 0 719.83 22.6 3 2 0 688.13 22.7 3 2 0 695.73 22.6 3 2 0 726.23 21.8 -4 -2 0 497.85 17 -4 -2 0 514.35 16.2 -4 -2 0 507.15 17.2 4 2 0 515.95 17.2 4 2 0 519.75 16.2 4 2 0 486.55 16.8 -5 -2 0 79.19 5.3 -5 -2 0 75.09 4.4 -5 -2 0 84.79 5.7 5 2 0 93.59 5.5 5 2 0 73.39 4.3 5 2 0 74.39 5.5 -6 -2 0 48.6 5.2 -6 -2 0 45.9 4.7 6 2 0 51.59 5.1 6 2 0 56.69 4.8 6 2 0 50.49 3.8 -7 -2 0 280.67 12.5 -7 -2 0 272.17 11.8 7 2 0 271.17 12.1 7 2 0 277.17 11.4 -8 -2 0 2.8 4.5 -8 -2 0 0.7 3.6 8 2 0 0.8 3.3 8 2 0 6.6 3.9 8 2 0 1.7 3.6 -9 -2 0 24.4 6.7 -9 -2 0 22.1 5.4 9 2 0 29.7 5.4 9 2 0 41.4 6.4 9 2 0 23.4 5.5 -10 -2 0 1.2 6.6 -10 -2 0 7.8 5 10 2 0 -5.9 4.8 10 2 0 -1.5 5.4 10 2 0 2.4 4.5 -11 -2 0 6.5 9.5 -11 -2 0 -6.9 6.1 11 2 0 3.1 5.2 11 2 0 4.3 6 -12 -2 0 3.9 7.2 12 2 0 6.1 6.5 12 2 0 -9.8 9.2 12 2 0 4 6.9 -13 -2 0 20.9 9.2 13 2 0 19.8 8.2 13 2 0 3.4 7.9 13 -3 0 5.5 6.4 -13 3 0 13.3 10.7 -13 3 0 9.3 7.9 12 -3 0 7.1 6.2 -12 3 0 -2.9 7.8 -12 3 0 -4.7 5.8 11 -3 0 0.9 5.4 -11 3 0 -8.9 4.2 -11 3 0 -4.4 5.9 10 -3 0 -6.6 4.4 -10 3 0 -2.1 5 -10 3 0 1.8 4 9 -3 0 9 4.6 -9 3 0 11 3.5 -9 3 0 9.8 4.6 8 -3 0 -0.6 2.9 8 -3 0 4.5 3.8 -8 3 0 0.7 3.2 -8 3 0 -0.6 2.5 7 -3 0 -1.5 1.1 7 -3 0 -2.1 2.9 7 -3 0 0.7 2.5 -7 3 0 -1.8 2 -7 3 0 -5.2 2.1 6 -3 0 48.3 4.3 6 -3 0 40.6 4.8 -6 3 0 48.5 3.9 5 -3 0 50.99 3.8 5 -3 0 48.5 4.3 -5 3 0 51.89 3.2 -5 3 0 51.09 3.2 4 -3 0 22.7 2.5 4 -3 0 15.9 2.8 -4 3 0 14.3 2.3 -4 3 0 16.6 1.7 -4 3 0 15.2 2 3 -3 0 136.89 5.3 3 -3 0 128.59 5.7 -3 3 0 115.59 4.3 -3 3 0 145.59 5.5 -3 3 0 128.29 4.2 -3 3 0 135.69 5.9 2 -3 0 12.2 1.5 2 -3 0 14 1.8 -2 3 0 15.5 1.5 -2 3 0 14.1 1.7 -2 3 0 14.5 1.9 1 -3 0 10.1 1.2 1 -3 0 8.6 1.3 -1 3 0 8.2 1.1 -1 3 0 11.5 1.6 -1 3 0 14.4 1.4 0 -3 0 0.8 0.6 0 -3 0 0.4 0.8 0 -3 0 0.5 0.4 0 -3 0 -0.5 0.9 0 3 0 1 0.8 0 3 0 0.6 0.4 0 3 0 0.6 0.6 -1 -3 0 83.69 3.7 -1 -3 0 77.49 3.4 1 3 0 77.19 3.4 1 3 0 76.09 3.7 -2 -3 0 20.5 1.1 -2 -3 0 19.4 2.1 -2 -3 0 25.7 2.4 2 3 0 25 2.4 2 3 0 17.6 1.1 2 3 0 16.4 2.1 -3 -3 0 34.8 3.1 -3 -3 0 34.8 3.2 -3 -3 0 39.7 2.1 3 3 0 32.6 3.1 3 3 0 34.3 3.3 3 3 0 33.2 1.9 -4 -3 0 3 1.5 -4 -3 0 6 2.4 -4 -3 0 4.6 2.1 4 3 0 5.6 2.4 4 3 0 5.3 1.5 4 3 0 6.9 2.3 -5 -3 0 165.98 6.9 -5 -3 0 162.18 8.2 -5 -3 0 163.28 7.9 5 3 0 160.88 8.1 5 3 0 171.98 7.9 5 3 0 155.78 6.5 -6 -3 0 3.5 2.7 -6 -3 0 1.9 2.6 -6 -3 0 4.3 3.2 6 3 0 5.8 3 6 3 0 0.1 2.8 -7 -3 0 21.6 5.1 -7 -3 0 20.3 4.2 7 3 0 19.9 4.6 7 3 0 23.4 4.2 -8 -3 0 1.4 3.6 -8 -3 0 -3 4.6 8 3 0 4 4.2 8 3 0 7.2 4.1 -9 -3 0 -2.4 5.7 -9 -3 0 1.1 4.6 9 3 0 2.1 5.4 9 3 0 9.6 4.5 9 3 0 -1 4.6 -10 -3 0 -1.2 6.9 -10 -3 0 -2.4 5.2 10 3 0 7.6 5.7 10 3 0 0.6 4.5 10 3 0 -12.2 5.7 -11 -3 0 0.6 6.1 -11 -3 0 3.9 8.7 11 3 0 2.3 5.2 11 3 0 9.8 7.2 11 3 0 -9.7 6.4 -12 -3 0 5.9 7.8 12 3 0 -3.6 8.7 12 3 0 -2.4 6.8 12 3 0 10 7.8 13 -4 0 1.1 6.8 -13 4 0 16.3 10 -13 4 0 -14.6 6.8 12 -4 0 -1.4 5.7 -12 4 0 10.8 7.8 -12 4 0 -5.6 5.3 11 -4 0 -1 5.9 -11 4 0 3.8 6 -11 4 0 3 4.6 10 -4 0 80.19 8.6 -10 4 0 82.89 8.5 -10 4 0 60.59 6.9 9 -4 0 60.89 7.6 9 -4 0 36.1 5.7 -9 4 0 41.5 5.4 -9 4 0 51.89 6.6 8 -4 0 23.3 4.2 8 -4 0 38.1 5.9 -8 4 0 31.2 4.4 -8 4 0 33.6 4.1 7 -4 0 56.69 5.5 7 -4 0 50.79 4.8 -7 4 0 55.79 4.5 -7 4 0 52.59 4 6 -4 0 7.6 2.8 6 -4 0 18.4 3.8 -6 4 0 15.3 2.3 -6 4 0 14.3 2.3 5 -4 0 0.2 2.1 5 -4 0 -0.2 1.7 -5 4 0 -1 1.2 -5 4 0 -2.4 1.1 4 -4 0 74.29 4.2 4 -4 0 79.99 4.8 -4 4 0 77.29 3 -4 4 0 70.49 2.9 -4 4 0 71.19 5.1 3 -4 0 1473.25 45.7 3 -4 0 1532.15 46.4 -3 4 0 1630.54 46.4 -3 4 0 1416.06 45.9 -3 4 0 1499.55 45.7 2 -4 0 359.46 12.2 2 -4 0 373.66 11.9 2 -4 0 375.86 12.5 -2 4 0 352.56 11.8 -2 4 0 353.26 12.1 -2 4 0 373.26 12.4 1 -4 0 2057.19 60.99 1 -4 0 2059.79 61.49 1 -4 0 1973.7 61.29 -1 4 0 2141.19 60.99 -1 4 0 2100.49 61.49 -1 4 0 2010.3 61.29 0 -4 0 133.69 5.1 0 -4 0 143.79 4.6 0 -4 0 134.19 5.4 0 -4 0 137.69 4.8 0 4 0 136.09 4.9 0 4 0 139.29 5.3 0 4 0 140.19 5.3 0 4 0 145.89 4.6 -1 -4 0 1475.95 44.7 -1 -4 0 1501.85 44.3 1 4 0 1454.05 44.6 1 4 0 1466.75 44.4 -2 -4 0 374.86 13 -2 -4 0 381.46 12.7 2 4 0 380.86 12.8 2 4 0 365.76 12.9 -3 -4 0 151.68 6.9 -3 -4 0 154.18 5.2 -3 -4 0 146.49 6.4 3 4 0 148.39 6.6 3 4 0 145.59 6.7 -4 -4 0 233.88 9.3 -4 -4 0 225.48 7.9 -4 -4 0 232.28 9.7 4 4 0 226.38 9.5 4 4 0 221.48 9.3 -5 -4 0 196.08 8.9 -5 -4 0 202.98 7.6 -5 -4 0 204.08 9.6 5 4 0 192.08 9.2 5 4 0 198.18 9 -6 -4 0 306.97 11.4 -6 -4 0 309.17 12.7 -6 -4 0 306.27 13.4 6 4 0 325.77 13.2 6 4 0 316.07 12.8 -7 -4 0 10.5 3.7 -7 -4 0 9.2 4.2 7 4 0 6.4 3.9 7 4 0 13 4.6 -8 -4 0 26.5 6.3 -8 -4 0 16.3 4.9 8 4 0 36.9 5.9 8 4 0 22.6 6.4 -9 -4 0 36.4 6.8 -9 -4 0 49.99 8 9 4 0 40.4 7.2 9 4 0 40.4 6 9 4 0 41 7 -10 -4 0 -1.1 7.5 -10 -4 0 5.3 10 10 4 0 -0.3 6.2 10 4 0 4 6.4 10 4 0 2.8 4.5 -11 -4 0 -1.3 6.4 -11 -4 0 23.4 10.7 11 4 0 4.7 7.4 11 4 0 10.7 5.5 11 4 0 4.4 7.8 -12 -4 0 0.6 8 12 4 0 8 9.9 12 4 0 -3.7 6.3 13 -5 0 -15.7 6.2 -13 5 0 -2.3 10.3 12 -5 0 -8.3 5.2 -12 5 0 -0.9 7.3 -12 5 0 -4.7 5 11 -5 0 9.1 6.3 -11 5 0 12.4 6.1 -11 5 0 9.8 4.8 10 -5 0 17.6 5.4 -10 5 0 25 4.6 9 -5 0 43.8 6.5 9 -5 0 56.19 7 -9 5 0 49.8 6.2 -9 5 0 46.5 5.2 8 -5 0 2 3.3 8 -5 0 -0.1 3.3 -8 5 0 0.9 2.9 -8 5 0 1.4 2.3 7 -5 0 6.9 3.2 7 -5 0 8.5 3.5 -7 5 0 10.8 2.6 6 -5 0 -1 2.1 6 -5 0 -3.1 2.3 -6 5 0 1.7 1.6 -6 5 0 0 1.3 5 -5 0 32 4.2 5 -5 0 38.8 3.4 -5 5 0 35 2.1 4 -5 0 36.9 3.7 4 -5 0 40.5 3.3 -4 5 0 34.5 3.4 3 -5 0 350.26 11.8 -3 5 0 342.07 11.8 -3 5 0 327.67 11.9 -3 5 0 344.47 12.5 2 -5 0 10.3 1.9 2 -5 0 6.7 1.6 2 -5 0 6.5 1.4 -2 5 0 8.6 1.6 -2 5 0 10.4 1.8 -2 5 0 13.6 2.3 1 -5 0 12.3 0.7 1 -5 0 11.7 1.4 1 -5 0 16.2 2.2 1 -5 0 14.7 1.9 -1 5 0 15.7 1.9 -1 5 0 13.4 1.6 -1 5 0 11.8 1 -1 5 0 14.2 2.1 -1 5 0 11.2 1.4 0 -5 0 65.99 2.6 0 -5 0 67.59 3.6 0 -5 0 68.79 2.9 0 -5 0 68.19 3.3 0 5 0 60.79 2.6 0 5 0 60.29 3.3 0 5 0 67.99 3.6 0 5 0 68.59 3 -1 -5 0 2.4 1.2 -1 -5 0 3.2 1.4 1 5 0 1.9 1.1 1 5 0 4 0.5 1 5 0 3.1 1.4 -2 -5 0 15.6 2.6 -2 -5 0 13.4 2.1 2 5 0 14.7 2.1 2 5 0 16.2 2.5 -3 -5 0 10.8 2.6 -3 -5 0 15 2.6 3 5 0 13.1 2.7 3 5 0 16.7 2.8 -4 -5 0 27.2 3.6 -4 -5 0 28.7 3.9 4 5 0 26.9 3.7 4 5 0 32.2 4.2 -5 -5 0 7.6 2.9 -5 -5 0 10.5 3.5 5 5 0 8.9 3 5 5 0 11.9 3.4 -6 -5 0 11.9 3.6 -6 -5 0 4.6 3.6 6 5 0 5 3.6 6 5 0 13.9 3.8 -7 -5 0 34.7 5.9 -7 -5 0 38.6 5.4 7 5 0 41.2 6 7 5 0 37.5 5.6 -8 -5 0 54.09 7.3 -8 -5 0 56.39 7.1 8 5 0 52.39 7.5 8 5 0 49.3 6.5 -9 -5 0 11.4 5.4 -9 -5 0 6.4 7.1 9 5 0 17.7 6 9 5 0 18.2 6.6 -10 -5 0 15.3 6.3 -10 -5 0 4.3 9.5 10 5 0 -0.9 4.5 10 5 0 11.6 7.6 10 5 0 -1.2 6.5 -11 -5 0 0 6.6 11 5 0 -7.6 5.3 -12 -5 0 -0.8 8.5 12 5 0 -10.4 11.2 12 5 0 -7.9 6.2 12 5 0 5.5 9.8 13 -6 0 20.8 8 -13 6 0 13.7 7.5 -13 6 0 4.8 9.5 12 -6 0 -4.6 5.5 -12 6 0 0.2 7 -12 6 0 6.1 5.4 11 -6 0 -6.5 5.1 -11 6 0 1.6 4.3 -11 6 0 2.9 5.8 10 -6 0 15.5 6.2 -10 6 0 11.8 3.9 -10 6 0 14.1 5 9 -6 0 12.4 4.8 9 -6 0 2.6 3.9 -9 6 0 5.5 2.9 -9 6 0 8.6 3.7 8 -6 0 2.8 3.8 8 -6 0 1.7 3.1 -8 6 0 -1.9 2.2 -8 6 0 -0.6 2.6 7 -6 0 4.1 3.1 7 -6 0 1.4 3.5 -7 6 0 -3.6 2 6 -6 0 63.29 5.6 6 -6 0 60.49 4.8 -6 6 0 66.89 3.4 -6 6 0 58.09 3.2 5 -6 0 -2.8 1.8 5 -6 0 -2.1 2 -5 6 0 -0.8 0.8 -5 6 0 -0.2 0.8 -5 6 0 -0.2 2.2 4 -6 0 26.8 3.2 -4 6 0 24.1 3.3 -3 6 0 13.5 2.4 2 -6 0 133.39 6.2 2 -6 0 136.79 5.6 2 -6 0 134.69 6.1 -2 6 0 139.99 6.4 -2 6 0 154.58 5.8 -2 6 0 137.69 4.4 -2 6 0 132.39 5.9 -2 6 0 145.09 4.5 1 -6 0 1.8 1 1 -6 0 1.8 0.6 1 -6 0 3.2 0.6 1 -6 0 3.7 1.5 1 -6 0 0.6 1.2 -1 6 0 2.8 0.8 -1 6 0 0.7 1.8 -1 6 0 1.6 1.4 -1 6 0 2.4 1.3 -1 6 0 5.2 1.3 0 -6 0 142.19 5.7 0 -6 0 137.09 6.1 0 -6 0 141.19 5.3 0 6 0 144.59 5.5 0 6 0 146.69 5 0 6 0 143.59 5.9 0 6 0 143.79 6.1 -1 -6 0 846.82 27.3 -1 -6 0 877.81 26.8 1 6 0 839.22 27 1 6 0 878.21 25.6 1 6 0 870.61 27.4 -2 -6 0 2167.88 65.79 -2 -6 0 2191.88 66.39 2 6 0 2180.48 66.09 2 6 0 2185.58 66.29 -3 -6 0 1451.35 46.3 -3 -6 0 1509.95 45.8 3 6 0 1468.95 46.1 3 6 0 1477.85 46 -4 -6 0 39.8 4.9 -4 -6 0 41.4 4.3 4 6 0 42.3 4.7 4 6 0 38.3 4.5 -5 -6 0 34.5 5 -5 -6 0 37.7 4.6 5 6 0 36.6 4.7 5 6 0 36.9 4.7 -6 -6 0 217.58 12 -6 -6 0 254.47 11.4 6 6 0 245.88 11.5 6 6 0 250.97 11.8 -7 -6 0 310.57 13.7 -7 -6 0 281.17 14.5 7 6 0 299.97 14.2 7 6 0 292.27 13.8 -8 -6 0 96.99 8.7 -8 -6 0 80.19 10.3 8 6 0 63.79 8.5 8 6 0 93.69 9.7 -9 -6 0 5.1 7.6 -9 -6 0 1.7 6.6 9 6 0 3.4 6.6 9 6 0 -2.5 5.5 -10 -6 0 25.7 9.7 -10 -6 0 15.7 6.8 10 6 0 17.9 10.8 10 6 0 5.9 5 -11 -6 0 -8.7 7.3 11 6 0 4.9 8.9 11 6 0 -4.3 5.1 11 6 0 7.3 8.9 -12 -6 0 2.5 9.3 12 6 0 -7.1 10.2 12 6 0 3.4 6.9 12 6 0 -14.3 12.5 13 -7 0 -5.7 6.1 -13 7 0 4.8 6.5 -13 7 0 -1.5 8.9 12 -7 0 -3.2 5.6 -12 7 0 4.2 7 -12 7 0 8.4 5.5 11 -7 0 8.7 6 -11 7 0 4.6 5.4 -11 7 0 2.2 4 10 -7 0 9 6.2 -10 7 0 6.3 4.3 -10 7 0 0.5 3.2 9 -7 0 -4.2 3.7 9 -7 0 2.8 4.4 -9 7 0 -0.6 2.6 8 -7 0 2.3 3.3 8 -7 0 -1.4 3.3 -8 7 0 -2.2 1.9 -8 7 0 0.5 2.5 7 -7 0 16.8 3.6 7 -7 0 7 3.5 -7 7 0 9.5 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2.9 6 0 2 9.1 2.4 6 0 2 8.3 2.4 6 0 2 9.5 2.9 6 0 2 10.4 2.8 -7 0 -2 197.38 9.7 7 0 2 188.48 8.7 7 0 2 194.28 9.1 7 0 2 192.58 8.4 7 0 2 191.18 9.2 -8 0 -2 50.29 7.4 -8 0 -2 50.29 6.1 8 0 2 49.7 5.9 8 0 2 41.6 5.1 8 0 2 50.89 5.6 8 0 2 55.59 5.2 -9 0 -2 24.5 5.2 -9 0 -2 28.2 6.2 9 0 2 28.8 5.3 9 0 2 21.4 4.5 9 0 2 21.7 5.2 9 0 2 31 4.9 -10 0 -2 6.4 6.4 -10 0 -2 6.5 4.9 10 0 2 1.5 4.6 10 0 2 1.3 4 10 0 2 -1.5 4.1 -11 0 -2 4.6 5.7 -11 0 -2 5.9 8.1 11 0 2 5.3 5.4 11 0 2 -0.4 5 11 0 2 6.5 4.5 -12 0 -2 13 10.7 -12 0 -2 21.8 7.4 12 0 2 27.8 5.4 12 0 2 42.1 7.6 12 0 2 22.2 6.1 -13 0 -2 8.2 8.5 13 0 2 -10.4 7 13 -1 -2 -8.8 6.6 -13 1 2 7.6 7.8 12 -1 -2 0.7 3.8 12 -1 -2 6.8 6.4 12 -1 -2 4.5 4.3 -12 1 2 2.7 9.2 -12 1 2 10.9 7.8 11 -1 -2 1.4 3.5 11 -1 -2 2.5 5.4 11 -1 -2 -10.1 4 -11 1 2 -9 4.9 -11 1 2 13.4 7.1 10 -1 -2 1 3.9 10 -1 -2 -1.9 4.8 10 -1 -2 0 3.2 -10 1 2 1.3 5.2 -10 1 2 -1 4.2 9 -1 -2 0.4 4.2 9 -1 -2 7.1 3.1 9 -1 -2 -2.4 3.3 -9 1 2 4.7 4.6 -9 1 2 0.7 3.5 8 -1 -2 -3.8 2.8 8 -1 -2 -2 3.4 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5 1 2 14.1 2.8 -6 -1 -2 20 3.9 6 1 2 19.3 3.5 6 1 2 19.4 3 6 1 2 23.3 3.5 6 1 2 18.4 3.2 -7 -1 -2 10.7 3.8 7 1 2 16.7 3.3 7 1 2 12.1 3.3 7 1 2 16.2 3.9 7 1 2 16.8 3.6 -8 -1 -2 3.7 3.8 -8 -1 -2 5.5 4.6 8 1 2 4.6 4.2 8 1 2 4.5 3.4 8 1 2 2.1 3.5 8 1 2 2.9 3.5 -9 -1 -2 26.6 5.7 -9 -1 -2 16.2 6.2 9 1 2 17.5 4.4 9 1 2 23.6 5.4 9 1 2 23.8 4.9 9 1 2 16.6 4.8 -10 -1 -2 1.7 4.8 -10 -1 -2 -0.6 6.2 10 1 2 8.7 5.2 10 1 2 -0.4 4.8 10 1 2 0.9 4.3 -11 -1 -2 5.1 8.5 -11 -1 -2 -10 6.6 11 1 2 3.6 5.6 11 1 2 6.1 5.1 11 1 2 3.8 6 -12 -1 -2 10.1 7.5 -12 -1 -2 -8.5 18.3 12 1 2 1.7 5.7 12 1 2 7.4 6.4 12 1 2 5.8 6.9 -13 -1 -2 -8.8 8.6 13 1 2 4.8 6.4 13 -2 -2 4.5 7.3 -13 2 2 -2.5 7.4 -13 2 2 0.9 11.4 12 -2 -2 12 6.7 -12 2 2 13.3 8.7 -12 2 2 10.4 6.2 11 -2 -2 5.6 2.8 11 -2 -2 6 2.8 11 -2 -2 9.8 6.1 -11 2 2 15.9 7 -11 2 2 13.5 5.5 10 -2 -2 70.59 5.2 10 -2 -2 79.49 8.7 10 -2 -2 79.49 5.6 -10 2 2 70.19 7.4 -10 2 2 85.39 9.4 9 -2 -2 8.3 4.3 9 -2 -2 2 2.4 9 -2 -2 0.9 2.7 -9 2 2 3.2 3.4 -9 2 2 5.1 5.3 8 -2 -2 -0.5 2.3 8 -2 -2 -3 3.7 8 -2 -2 -2 2.1 -8 2 2 -3 2.5 -8 2 2 -4 3.2 7 -2 -2 15.5 3.8 7 -2 -2 14.4 2.5 7 -2 -2 17.1 2.8 -7 2 2 14.6 3.3 -7 2 2 11.6 2.7 6 -2 -2 634.44 20.9 6 -2 -2 711.93 21.3 6 -2 -2 670.93 23.1 -6 2 2 649.34 21.5 -6 2 2 669.93 21.7 5 -2 -2 -0.6 1.3 5 -2 -2 1.5 1.4 5 -2 -2 0.1 2.1 -5 2 2 -0.8 1.4 -5 2 2 -1.4 1.6 4 -2 -2 115.19 4.2 4 -2 -2 111.79 5.7 4 -2 -2 96.29 4.2 -4 2 2 111.79 4.4 -4 2 2 112.19 5.1 -4 2 2 107.29 4.4 3 -2 -2 456.75 14.6 3 -2 -2 429.46 13.1 3 -2 -2 394.76 13.1 -3 2 2 410.46 13.3 -3 2 2 449.76 14 2 -2 -2 390.06 12 2 -2 -2 429.86 13.2 -2 2 2 412.36 12.6 -2 2 2 380.06 12 -2 2 2 362.96 12.2 1 -2 -2 1495.95 40 1 -2 -2 1393.86 39.5 1 -2 -2 1321.67 39.4 -1 2 2 1308.47 39.5 -1 2 2 1154.58 39.8 -1 2 2 1300.87 39.4 -1 2 2 1347.17 39.5 0 -2 -2 303.57 9.5 0 2 2 293.47 9.6 0 2 2 246.78 8.7 -1 -2 -2 1869.91 54.79 -1 -2 -2 1819.62 54.79 1 2 2 1844.12 54.79 1 2 2 1798.52 54.89 -2 -2 -2 2014 61.79 -2 -2 -2 2075.79 61.69 2 2 2 2020.1 61.69 2 2 2 2062.99 61.69 2 2 2 2103.99 60.89 -3 -2 -2 878.31 27.4 -3 -2 -2 858.31 27.5 3 2 2 839.12 27.2 3 2 2 860.41 27.4 3 2 2 892.61 26.4 -4 -2 -2 190.88 8 -4 -2 -2 182.18 8.2 4 2 2 194.08 7 4 2 2 184.18 8.2 4 2 2 186.98 8 -5 -2 -2 3410.26 106.49 -5 -2 -2 3645.54 105.59 -5 -2 -2 3614.24 106.39 5 2 2 3608.14 106.49 5 2 2 3450.05 105.89 5 2 2 3501.85 105.19 -6 -2 -2 61.49 5.7 6 2 2 58.79 4.9 6 2 2 60.39 4.5 6 2 2 57.79 4.2 6 2 2 61.79 5.7 -7 -2 -2 67.09 6.3 -7 -2 -2 80.29 7.2 7 2 2 83.79 5.3 7 2 2 75.89 5.4 7 2 2 71.09 6.7 7 2 2 71.19 6 -8 -2 -2 265.67 12.7 -8 -2 -2 296.87 14 8 2 2 256.57 11.9 8 2 2 284.07 12.2 8 2 2 281.97 13.1 8 2 2 284.37 11.7 -9 -2 -2 -2.2 4.4 -9 -2 -2 6 6 9 2 2 -3.5 3.7 9 2 2 0.4 3.5 9 2 2 4 5 9 2 2 5.5 4.7 -10 -2 -2 15.2 7.2 -10 -2 -2 6.2 5.4 10 2 2 8.6 4.4 10 2 2 22.9 6.2 10 2 2 -1.9 5.1 -11 -2 -2 6.3 6.5 -11 -2 -2 7.4 9 11 2 2 1.7 5.2 11 2 2 -7.5 6 -12 -2 -2 5.6 7.6 12 2 2 0.6 7.2 12 2 2 6.9 6.2 12 2 2 11.9 9.8 13 -3 -2 -3.3 6.4 -13 3 2 17.5 10.3 -13 3 2 -1.5 7.1 12 -3 -2 -1.1 6.1 -12 3 2 -9.2 7.7 -12 3 2 0.8 5.7 -11 3 2 2.1 4.9 -11 3 2 16.4 6.4 10 -3 -2 10.8 5.2 -10 3 2 11.2 5.5 -10 3 2 13.6 4.4 9 -3 -2 15.9 5 -9 3 2 14.9 4.6 -9 3 2 15.3 3.9 8 -3 -2 8.2 4 8 -3 -2 5.1 1.8 8 -3 -2 6.7 1.9 -8 3 2 6.5 2.9 -8 3 2 3.2 3.5 7 -3 -2 2.1 3.2 -7 3 2 -3.9 2.4 -7 3 2 -1.6 2 6 -3 -2 40.3 5 6 -3 -2 32.6 2.3 -6 3 2 34.8 3.5 -6 3 2 40.5 3.2 5 -3 -2 360.66 12 5 -3 -2 388.26 14.7 -5 3 2 395.16 12.8 -5 3 2 421.46 13 4 -3 -2 7.9 2.2 -4 3 2 12.9 1.6 -4 3 2 10.7 2.3 -4 3 2 11.9 1.5 3 -3 -2 1318.67 40.6 -3 3 2 1432.66 40.1 -3 3 2 1166.98 39.2 -3 3 2 1352.56 39.1 2 -3 -2 4.9 1.6 -2 3 2 4.4 0.8 -2 3 2 8.1 1.8 -2 3 2 5.2 1 -2 3 2 5.3 1.3 -2 3 2 6.1 0.7 1 -3 -2 15.7 1.7 1 -3 -2 15.4 1.1 1 -3 -2 13.2 1.1 1 -3 -2 17.7 1.5 -1 3 2 13.7 1.3 -1 3 2 16.5 1.5 -1 3 2 16.5 1.4 -1 3 2 17.1 1.9 0 -3 -2 117.39 4.4 0 -3 -2 92.79 4 0 -3 -2 106.29 3.9 0 3 2 94.99 4.1 0 3 2 116.39 4.5 0 3 2 99.69 3.9 -1 -3 -2 8.5 1.5 -1 -3 -2 12.6 2 1 3 2 7.8 1.6 1 3 2 7.9 1.4 -2 -3 -2 6.8 1.8 -2 -3 -2 4.9 1.5 2 3 2 4.3 1.7 2 3 2 6.5 1 2 3 2 5.5 1.6 -3 -3 -2 13.9 2.5 -3 -3 -2 13.3 2.4 3 3 2 15.4 2.4 3 3 2 16.5 1.6 3 3 2 13.9 2.5 -4 -3 -2 239.38 10.2 -4 -3 -2 250.97 10 4 3 2 252.27 10 4 3 2 239.38 10.1 4 3 2 238.48 8.5 -5 -3 -2 1.7 2.8 5 3 2 0.3 2.8 5 3 2 5.8 1.8 5 3 2 1.6 2.7 -6 -3 -2 -0.6 2.6 -6 -3 -2 7.6 3.5 6 3 2 3.7 3.2 6 3 2 1.2 2.9 6 3 2 -0.1 1.9 -7 -3 -2 13.5 5.6 -7 -3 -2 26.6 4.7 7 3 2 26.9 3.7 7 3 2 19.2 3.7 7 3 2 28 4.8 7 3 2 26.6 5 -8 -3 -2 120.39 8.8 -8 -3 -2 111.79 9.9 8 3 2 107.19 7.2 8 3 2 118.19 9.3 8 3 2 119.19 7.1 8 3 2 120.79 8.5 -9 -3 -2 9.3 5 -9 -3 -2 16.8 6.4 9 3 2 1.6 4.9 9 3 2 6.5 3.9 -10 -3 -2 9.8 7.9 -10 -3 -2 -1.4 6.1 10 3 2 -1.7 4.3 10 3 2 3.5 5.8 10 3 2 6.9 6.4 -11 -3 -2 11.7 9.8 -11 -3 -2 -1.8 6.6 11 3 2 -2.7 6.9 11 3 2 7.7 7.5 11 3 2 3.9 5.5 -12 -3 -2 -8.4 7.8 12 3 2 4.9 6.1 12 3 2 5.4 9.2 12 3 2 -7.2 8.4 13 -4 -2 14.8 7.3 -13 4 2 8.9 7.1 -13 4 2 9.6 9.5 12 -4 -2 11.6 5.9 -12 4 2 8.4 8.2 -12 4 2 -1.1 5.5 11 -4 -2 4.1 6.2 -11 4 2 4.3 4.6 -11 4 2 2.4 6.2 10 -4 -2 70.19 8.9 -10 4 2 86.69 8.7 -10 4 2 78.89 6.9 9 -4 -2 34.5 5.9 -9 4 2 27.5 4.2 -9 4 2 30 5.2 8 -4 -2 95.49 7.9 -8 4 2 100.69 6.6 -8 4 2 102.49 6 7 -4 -2 13.5 3.7 -7 4 2 9.8 2.5 -7 4 2 10 3 6 -4 -2 263.87 11.5 -6 4 2 263.27 9.4 -6 4 2 260.27 9.3 5 -4 -2 198.58 9 -5 4 2 188.38 6.9 -5 4 2 195.68 7 4 -4 -2 984.2 30.1 -4 4 2 910.01 28 -4 4 2 892.21 27.9 3 -4 -2 334.27 11.9 -3 4 2 303.57 10.9 -3 4 2 341.37 11.2 -3 4 2 340.97 11.9 -3 4 2 316.97 10.1 -3 4 2 314.07 9.9 2 -4 -2 465.75 15.5 2 -4 -2 459.35 14.9 -2 4 2 491.85 15.6 -2 4 2 459.45 14.2 -2 4 2 459.45 14.7 -2 4 2 465.95 14.9 -2 4 2 457.85 14.1 1 -4 -2 191.18 7.1 1 -4 -2 198.58 6.9 1 -4 -2 194.18 6.5 1 -4 -2 199.28 6.3 -1 4 2 171.58 6.9 -1 4 2 202.18 6.6 -1 4 2 208.68 7.2 -1 -4 -2 175.88 7.1 -1 -4 -2 185.78 6.9 1 4 2 173.98 7.1 1 4 2 185.58 6.2 1 4 2 177.78 6.9 -2 -4 -2 75.29 4.4 -2 -4 -2 77.89 4.2 2 4 2 67.49 4.1 2 4 2 74.59 4.4 -3 -4 -2 704.63 24.1 3 4 2 709.33 23.9 3 4 2 735.23 23.9 3 4 2 758.02 22.1 -4 -4 -2 3.3 2.5 4 4 2 5.8 2.7 4 4 2 1.5 1.2 4 4 2 -4.2 2.1 -5 -4 -2 114.89 6.8 -5 -4 -2 113.69 7.4 5 4 2 115.39 7 5 4 2 116.39 7.2 5 4 2 123.79 5.2 -6 -4 -2 115.29 7.5 -6 -4 -2 110.99 8 6 4 2 131.79 8.1 6 4 2 118.19 5.8 6 4 2 126.79 7.7 -7 -4 -2 245.08 12.5 -7 -4 -2 227.58 11.4 7 4 2 223.28 11.1 7 4 2 250.47 12.3 7 4 2 225.48 9.5 -8 -4 -2 265.27 13 -8 -4 -2 267.67 14.3 8 4 2 251.67 11.3 8 4 2 264.87 12.8 -9 -4 -2 43.2 7.8 -9 -4 -2 45.9 7.4 9 4 2 31.8 6.2 9 4 2 36.1 7.4 9 4 2 43.6 5.7 -10 -4 -2 22.6 8.9 -10 -4 -2 10.5 6.1 10 4 2 26.5 7.3 10 4 2 28.3 7.2 10 4 2 16.9 5.1 -11 -4 -2 38.7 12 -11 -4 -2 26.6 7.9 11 4 2 17.1 8.7 11 4 2 10.6 7.7 11 4 2 22.7 6.1 -12 -4 -2 20.2 8.3 12 4 2 -8.3 6 12 4 2 0.8 11.7 12 4 2 14.1 11.8 13 -5 -2 4.7 6.5 -13 5 2 8.3 9.5 -13 5 2 -13.1 9.8 12 -5 -2 -5.7 5.6 -12 5 2 2.3 5.5 -12 5 2 13.2 7.6 11 -5 -2 6.5 5.9 -11 5 2 1.8 5.7 -11 5 2 -2.1 4.4 10 -5 -2 -3.6 4.9 -10 5 2 13.7 7.3 -10 5 2 6.2 3.5 9 -5 -2 2.7 4.5 -9 5 2 2.6 3.8 -9 5 2 -2.7 2.6 8 -5 -2 5.4 3.8 -8 5 2 7.2 2.6 -8 5 2 7.1 3.3 7 -5 -2 21.2 4.4 -7 5 2 19.7 3.1 -7 5 2 20 2.7 6 -5 -2 -3.6 2.3 -6 5 2 4.9 1.5 -6 5 2 7.4 1.8 5 -5 -2 325.97 13.5 -5 5 2 354.86 11.1 -5 5 2 352.66 11.2 4 -5 -2 9.2 2.5 -4 5 2 7.2 1.1 -4 5 2 6 1.8 -4 5 2 7.1 0.9 3 -5 -2 49.7 3.8 -3 5 2 45.8 4.1 -3 5 2 60.69 3.2 -3 5 2 45.1 3.3 -3 5 2 57.49 2 -3 5 2 46.7 2.1 2 -5 -2 70.59 3.5 2 -5 -2 59.99 3.8 -2 5 2 61.59 3.4 -2 5 2 55.79 2.6 -2 5 2 68.79 3.4 -2 5 2 67.69 2.7 -2 5 2 72.09 4.2 1 -5 -2 28.2 2.6 1 -5 -2 39.1 2.6 -1 5 2 30.2 2.5 -1 5 2 34.7 2.1 -1 5 2 35.8 2.8 0 -5 -2 1.3 1 0 -5 -2 0.5 1.4 0 5 2 0.1 1 0 5 2 0.9 1.4 0 5 2 1.2 1.2 -1 -5 -2 258.37 9.3 -1 -5 -2 271.17 9.7 1 5 2 268.77 8.8 1 5 2 241.98 9.6 1 5 2 242.78 9.3 -2 -5 -2 0.2 1.8 -2 -5 -2 0.7 1.5 2 5 2 1.1 1.7 2 5 2 -0.9 1.7 -3 -5 -2 57.59 4.3 -3 -5 -2 56.49 4.6 3 5 2 57.49 4.5 3 5 2 58.99 4.7 3 5 2 51.89 2.5 -4 -5 -2 -1 2.4 -4 -5 -2 -0.5 2.3 4 5 2 1.3 1.2 4 5 2 -2.9 2.4 4 5 2 1.4 2.6 -5 -5 -2 17 4.3 -5 -5 -2 13.9 3.5 5 5 2 20.5 3.9 5 5 2 12.9 2.1 5 5 2 20.1 4 -6 -5 -2 4.5 7.3 -6 -5 -2 2.9 3.3 6 5 2 3.5 3.6 6 5 2 2.5 3.4 6 5 2 2.9 2 -7 -5 -2 13.8 4.5 -7 -5 -2 6.9 5 7 5 2 12.4 2.9 7 5 2 15.7 4.8 -8 -5 -2 15.9 6.3 -8 -5 -2 1.8 4.4 8 5 2 14.3 5.2 8 5 2 14.3 3.7 8 5 2 9.4 5.8 -9 -5 -2 2.8 5.1 -9 -5 -2 -1.5 6.6 9 5 2 4.7 5.7 9 5 2 3.7 4.1 9 5 2 4.6 6 -10 -5 -2 9.8 6.3 -10 -5 -2 11.3 8.6 10 5 2 1.5 6.7 10 5 2 11.3 4.8 10 5 2 -4.4 7.2 -11 -5 -2 -1.7 7.2 11 5 2 6.9 8.8 11 5 2 -3.1 5.3 -12 -5 -2 7.3 8.8 12 5 2 0.2 6.2 12 5 2 -3.3 11.4 12 5 2 8.9 10.2 13 -6 -2 3.3 7.1 -13 6 2 20.3 9.7 -13 6 2 10.6 7.1 12 -6 -2 25.2 7.3 -12 6 2 49 8.4 -12 6 2 48 6.9 11 -6 -2 0.8 6.1 -11 6 2 4.7 5.7 -11 6 2 -2.3 4.2 10 -6 -2 26 6.6 -10 6 2 42.4 6 -10 6 2 40.7 4.9 9 -6 -2 5.5 4.8 -9 6 2 1.2 3.6 -9 6 2 2.8 2.6 8 -6 -2 21.3 5 -8 6 2 24.2 3.2 -8 6 2 25.6 3.9 7 -6 -2 420.46 16.9 -7 6 2 405.06 13.7 -7 6 2 395.96 13.5 6 -6 -2 176.38 9.1 -6 6 2 172.18 8.4 -6 6 2 169.88 6.3 -6 6 2 169.58 6.5 5 -6 -2 75.59 5.5 -5 6 2 72.79 3 -5 6 2 71.09 4.7 -5 6 2 67.09 3.2 4 -6 -2 208.08 9 -4 6 2 195.08 7.9 -4 6 2 197.58 6.3 -4 6 2 195.28 6.5 3 -6 -2 64.19 3.9 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3 -0.6 6.1 8 10 -3 -0.9 6.5 8 10 -3 0.4 6.6 -8 -10 3 -1.1 5.4 -8 -10 3 -0.5 8.6 7 10 -3 1.1 5.7 -7 -10 3 12.9 5.2 6 10 -3 8.1 5.8 6 10 -3 2.3 5.2 -6 -10 3 2 5.4 -6 -10 3 9.1 4.8 5 10 -3 19.1 5.3 5 10 -3 22.8 4.9 -5 -10 3 29.7 5 -5 -10 3 15.6 5.2 4 10 -3 12.3 4.5 -4 -10 3 9.3 3.4 -4 -10 3 5.1 4.2 3 10 -3 -0.4 2.6 3 10 -3 0 3.2 -3 -10 3 -0.8 2.4 -3 -10 3 2.2 3.2 2 10 -3 74.89 5.4 2 10 -3 65.79 5.8 -2 -10 3 72.69 6 -2 -10 3 74.69 5.2 -2 -10 3 73.49 6.5 1 10 -3 4.4 2.3 1 10 -3 4.4 2.7 -1 -10 3 1.1 3.1 -1 -10 3 4.2 2.4 -1 -10 3 -0.2 2 -1 -10 3 0.9 1.2 0 10 -3 26.3 3.4 0 10 -3 28.4 3.1 0 -10 3 27.8 4.3 0 -10 3 30.6 2.9 0 -10 3 27.2 2.5 0 -10 3 30.1 3.6 -1 10 -3 41.9 3.1 -1 10 -3 42.8 4.5 -1 10 -3 40.3 3.7 -1 10 -3 38.1 4.3 1 -10 3 36.3 4.3 1 -10 3 44.9 2.5 1 -10 3 39.8 3.1 -2 10 -3 7.1 1.6 -2 10 -3 9.6 3 -2 10 -3 5.9 1.9 2 -10 3 5 2.8 2 -10 3 5.4 2.1 -3 10 -3 5.4 3.2 -3 10 -3 5.7 1.2 -3 10 -3 4.1 1.6 3 -10 3 1.4 3.1 3 -10 3 7.1 2.6 -4 10 -3 -3.3 2.6 4 -10 3 -0.9 2.2 -5 10 -3 -0.3 3.3 5 -10 3 1.7 3.1 5 -10 3 3.8 2.8 -6 10 -3 3.2 3.8 6 -10 3 -3.2 2.6 6 -10 3 -0.2 3.4 -7 10 -3 27.1 5.5 -7 10 -3 20.9 2.3 -7 10 -3 24 2.2 7 -10 3 22 4.9 7 -10 3 23.2 4.6 -8 10 -3 -2 2.2 -8 10 -3 -9.8 5 -8 10 -3 0.1 2.1 8 -10 3 0.8 4.5 -9 10 -3 -1.2 2.7 -9 10 -3 2.1 6.7 -9 10 -3 3.4 3.2 9 -10 3 0.7 5 -10 10 -3 3.9 4 -10 10 -3 -4.8 8.3 10 -10 3 3.4 5.1 10 -10 3 5.7 5.9 -11 10 -3 4.8 5.5 -11 10 -3 19.6 10.4 -11 10 -3 2.8 3.9 11 -10 3 -0.4 6.3 11 -10 3 0.4 5.3 -12 10 -3 1.9 5.1 -12 10 -3 2.9 12.4 -12 10 -3 -0.5 7 12 -10 3 0.1 6.6 11 9 -3 -11 14.5 11 9 -3 -17.9 10.3 -11 -9 3 -3.1 8.3 10 9 -3 34.8 9.9 10 9 -3 30.1 10.1 -10 -9 3 49.5 8.4 9 9 -3 36.6 8.3 9 9 -3 23.7 8 -9 -9 3 31.1 7.1 -9 -9 3 29.5 9.1 8 9 -3 -7 5.7 7 9 -3 140.59 10.9 7 9 -3 172.08 11.5 -7 -9 3 150.08 10.2 6 9 -3 509.25 20.4 6 9 -3 512.15 20.2 -6 -9 3 511.45 19.5 -6 -9 3 506.65 20.9 5 9 -3 428.86 17.4 5 9 -3 451.05 17.6 -5 -9 3 427.96 18 -5 -9 3 455.55 17 4 9 -3 -1.7 3.4 -4 -9 3 -0.4 3.4 -4 -9 3 5.4 2.8 3 9 -3 473.25 17.2 3 9 -3 469.85 17.4 -3 -9 3 472.55 17.7 -3 -9 3 474.35 16.8 2 9 -3 332.97 13.1 2 9 -3 326.67 12.5 -2 -9 3 329.17 10.1 -2 -9 3 344.97 13.7 -2 -9 3 326.77 13 -2 -9 3 336.37 12.3 1 9 -3 2763.52 83.09 1 9 -3 2792.02 82.69 -1 -9 3 2680.13 83.79 -1 -9 3 2715.83 81.19 -1 -9 3 2781.92 82.49 -1 -9 3 2778.42 83.09 0 9 -3 390.26 13 0 9 -3 380.26 13.4 0 -9 3 373.66 13.1 0 -9 3 368.76 12.7 0 -9 3 382.06 14.4 0 -9 3 379.56 12.4 -1 9 -3 11.4 2.9 -1 9 -3 10.7 1.8 -1 9 -3 8.9 2 -1 9 -3 15.1 3 1 -9 3 6.9 2.8 1 -9 3 14.4 2.2 -2 9 -3 208.98 9.3 -2 9 -3 212.58 7.6 -2 9 -3 208.28 7.3 2 -9 3 212.28 9.6 2 -9 3 210.58 8.2 -3 9 -3 276.87 8.5 -3 9 -3 257.87 8.4 -3 9 -3 265.07 11 3 -9 3 264.87 10.2 3 -9 3 245.08 11.1 -4 9 -3 48.4 4.8 4 -9 3 55.29 4.6 4 -9 3 54.29 5.2 -5 9 -3 566.14 20.5 5 -9 3 552.64 19.7 5 -9 3 567.84 20.9 -6 9 -3 656.73 23.9 6 -9 3 681.43 24.3 6 -9 3 643.84 23.1 -7 9 -3 -1.3 1.7 -7 9 -3 3.4 1.7 7 -9 3 -1.5 3.8 7 -9 3 -0.7 3.1 -8 9 -3 73.49 8.4 -8 9 -3 60.99 4.3 -8 9 -3 64.39 4.6 8 -9 3 57.29 6.5 8 -9 3 57.49 7.4 -9 9 -3 48 5.5 -9 9 -3 66.99 9.3 -9 9 -3 46.1 4.8 9 -9 3 56.69 8.1 9 -9 3 47.1 7.1 -10 9 -3 118.39 8.3 -10 9 -3 106.39 12.8 10 -9 3 127.79 10 10 -9 3 114.19 10.9 -11 9 -3 -9.1 9.6 -11 9 -3 4.1 4.1 11 -9 3 -2.3 5.3 11 -9 3 -7.1 5.3 -12 9 -3 1.1 7.2 -12 9 -3 6.2 12.5 -12 9 -3 -0.1 5.3 12 -9 3 5 7.4 -13 9 -3 -5.7 6.7 -13 9 -3 29 10 13 -9 3 2.6 7.5 11 8 -3 16.8 10.2 11 8 -3 11.3 10.4 -11 -8 3 16.6 8.9 10 8 -3 -7.3 8.4 10 8 -3 -8.5 8.1 -10 -8 3 -2.4 6.2 -10 -8 3 10.9 10.3 9 8 -3 -0.7 8.4 -9 -8 3 3.5 5.7 -9 -8 3 -14.9 7.5 8 8 -3 15.3 5.8 8 8 -3 8.9 5.7 -8 -8 3 6.4 5.5 7 8 -3 16.5 5.4 7 8 -3 21.4 5.9 -7 -8 3 13.9 5.2 6 8 -3 59.49 7.3 6 8 -3 51.49 6.5 -6 -8 3 63.19 8 -6 -8 3 55.59 6.6 5 8 -3 14.2 4.2 5 8 -3 16.4 4.1 -5 -8 3 20.5 4.6 -5 -8 3 15 3.7 4 8 -3 -4.2 2.7 -4 -8 3 0 2.4 -4 -8 3 -0.4 2.9 3 8 -3 17.4 3.3 3 8 -3 14.9 3.7 -3 -8 3 16.2 3.5 -3 -8 3 14.1 2.9 2 8 -3 20.8 3.9 2 8 -3 24 3.2 -2 -8 3 26.1 3.4 -2 -8 3 23.6 1.3 -2 -8 3 19.5 3.3 -2 -8 3 32.7 4.4 1 8 -3 76.09 4.9 1 8 -3 72.09 4.3 -1 -8 3 71.99 3.1 -1 -8 3 72.39 5.2 -1 -8 3 74.19 4.7 -1 -8 3 73.99 4.2 0 8 -3 20.8 2.8 0 8 -3 18.7 2.3 0 8 -3 23.3 3.3 0 -8 3 23.6 2.3 0 -8 3 22.4 2 0 -8 3 23 3.5 0 -8 3 22.1 2.6 -1 8 -3 0.5 1.3 -1 8 -3 1.1 1.1 -1 8 -3 4.9 2 -1 8 -3 0.7 1.8 1 -8 3 3.7 2.2 1 -8 3 0.7 1 1 -8 3 0.2 1.4 1 -8 3 1.7 0.9 -2 8 -3 29.8 3.5 -2 8 -3 22.9 3 -2 8 -3 26.3 1.9 -2 8 -3 24.9 3.4 2 -8 3 25.1 2.9 2 -8 3 32 4.1 -3 8 -3 11.8 3 3 -8 3 11.3 2.6 3 -8 3 11.3 3.5 -4 8 -3 0.8 2.5 4 -8 3 2.8 2.6 4 -8 3 3.8 2.3 -5 8 -3 3.8 3.2 5 -8 3 4.6 3.1 5 -8 3 7.4 2.7 -6 8 -3 0.6 3.5 -6 8 -3 0.6 1.3 -6 8 -3 -0.1 1.3 6 -8 3 -0.5 3.1 6 -8 3 0.4 2.6 -7 8 -3 9.2 2.3 -7 8 -3 7 2.1 -7 8 -3 5.3 4.3 7 -8 3 5.4 3.5 7 -8 3 4.7 3.4 -8 8 -3 3.4 2.4 -8 8 -3 -1.3 2.2 -8 8 -3 -6.5 5.2 8 -8 3 0.2 3.4 8 -8 3 -8.6 3.7 -9 8 -3 45.2 8.9 -9 8 -3 40.2 4.9 -9 8 -3 41.9 5.5 9 -8 3 32.5 6.5 9 -8 3 38.1 6.5 -10 8 -3 3.9 4.4 10 -8 3 8.4 5.2 -11 8 -3 -2.1 4.1 -11 8 -3 11.1 5.8 11 -8 3 -6.6 4.7 11 -8 3 0.5 5.5 -12 8 -3 -6.9 7.4 -12 8 -3 5.7 5.4 12 -8 3 -8.4 5.7 -13 8 -3 7.1 9.8 -13 8 -3 1 6.9 13 -8 3 2.3 7.5 12 7 -3 40.9 13.3 12 7 -3 11.9 7.2 12 7 -3 0.7 11.4 -12 -7 3 14.3 9.7 11 7 -3 6.1 9.2 11 7 -3 2.6 9.8 -11 -7 3 2.5 7.4 10 7 -3 -6 7.6 10 7 -3 3.3 8.5 -10 -7 3 -1.2 9.1 -10 -7 3 13.8 6.6 9 7 -3 -0.6 6.6 9 7 -3 9.9 6.3 -9 -7 3 9.8 7.6 -9 -7 3 -7.4 5.1 8 7 -3 164.58 11.1 8 7 -3 150.48 10.9 -8 -7 3 161.58 8.7 -8 -7 3 168.58 10.6 7 7 -3 3.2 4.1 7 7 -3 5.3 4.8 -7 -7 3 3.3 4.1 -7 -7 3 7.4 5.1 -7 -7 3 2.5 2.9 6 7 -3 103.69 7.9 6 7 -3 101.29 9 -6 -7 3 110.69 7.5 -6 -7 3 106.69 4.8 -6 -7 3 104.09 8.6 5 7 -3 51.59 5.4 5 7 -3 47.7 5.7 -5 -7 3 52.49 6 -5 -7 3 46.9 2.7 -5 -7 3 44.9 5 4 7 -3 388.66 15 4 7 -3 412.26 15 -4 -7 3 387.96 15.2 -4 -7 3 402.56 12.2 -4 -7 3 402.66 14.7 3 7 -3 1 2.2 3 7 -3 0.3 2.3 -3 -7 3 -0.1 1.9 -3 -7 3 1.3 2.4 2 7 -3 10.7 2.6 2 7 -3 10.9 2.4 -2 -7 3 11 2.4 -2 -7 3 11.9 1.1 -2 -7 3 9.1 2.6 1 7 -3 20.3 2.4 1 7 -3 22.8 2.9 -1 -7 3 21.2 2.8 -1 -7 3 22.1 2.4 -1 -7 3 20 1.6 -1 -7 3 22.1 3.2 0 7 -3 323.67 11.7 0 7 -3 311.27 10.9 0 7 -3 313.37 10.6 0 -7 3 305.87 11.6 0 -7 3 315.77 10.8 0 -7 3 305.77 10.4 0 -7 3 319.37 10.3 -1 7 -3 45.7 2.5 -1 7 -3 42.5 3.6 -1 7 -3 41.5 2.8 -1 7 -3 45.7 4.9 -1 7 -3 43.7 3.4 1 -7 3 45.3 2.8 1 -7 3 43.8 3.7 1 -7 3 42.6 2 -2 7 -3 581.04 17.2 -2 7 -3 556.44 19.1 -2 7 -3 564.84 17.2 -2 7 -3 559.54 18.6 2 -7 3 565.04 18.3 2 -7 3 557.34 19.3 -3 7 -3 340.17 13.3 3 -7 3 375.96 12.9 3 -7 3 368.56 13.6 -4 7 -3 5.4 2.8 4 -7 3 4.5 2.3 4 -7 3 4.4 2.3 -5 7 -3 30.3 4.3 -5 7 -3 28.9 1.5 -5 7 -3 28.7 1.7 5 -7 3 27.9 3.8 5 -7 3 35.7 4.9 -6 7 -3 7.5 1.6 -6 7 -3 11.7 4.2 -6 7 -3 7.5 1.9 6 -7 3 4 3 6 -7 3 9.5 3.3 -7 7 -3 97.69 5.1 -7 7 -3 100.69 5.1 7 -7 3 94.79 7.3 7 -7 3 98.29 6.7 -8 7 -3 19.2 3.3 -8 7 -3 17.4 3.1 8 -7 3 15 4.6 8 -7 3 14 4.5 -9 7 -3 109.79 7.3 -9 7 -3 105.09 6.6 9 -7 3 107.69 15 9 -7 3 103.79 9.1 -10 7 -3 58.49 7.4 10 -7 3 45.7 7.6 10 -7 3 42.6 6.9 -11 7 -3 2.1 4.6 -11 7 -3 -0.4 6 11 -7 3 9.5 6.1 11 -7 3 1.9 5.3 -12 7 -3 3.3 7.8 -12 7 -3 2.3 5.6 12 -7 3 2.2 5.8 -13 7 -3 19.8 10.3 -13 7 -3 -10.3 6.8 13 -7 3 -6.8 6.8 12 6 -3 -1.5 6.9 12 6 -3 5.5 11.7 12 6 -3 -3.5 10 -12 -6 3 5.6 8.6 11 6 -3 -4 8.1 11 6 -3 20.2 8.7 -11 -6 3 -1.2 6.7 10 6 -3 0.6 7.1 10 6 -3 0.2 8.7 -10 -6 3 4.2 6.2 -10 -6 3 -11 7.9 9 6 -3 -1.1 5.6 9 6 -3 -5 5.7 -9 -6 3 -6.8 4.7 -9 -6 3 -17 6.1 8 6 -3 18.9 5.8 8 6 -3 34.5 6.3 -8 -6 3 34 6.9 -8 -6 3 26.8 5.6 7 6 -3 10 4.5 7 6 -3 2.1 4.1 -7 -6 3 4.7 4.6 -7 -6 3 -1.3 3 -7 -6 3 7.7 4.1 6 6 -3 7.8 3.7 6 6 -3 14.6 4.2 -6 -6 3 3.2 2.3 -6 -6 3 6.3 3.5 5 6 -3 -1.7 2.5 5 6 -3 -4.9 2.6 -5 -6 3 0.7 3 -5 -6 3 -1.1 2.4 -5 -6 3 0.2 1.6 4 6 -3 -2.6 2.3 4 6 -3 -4.4 2 -4 -6 3 -1.8 2.4 -4 -6 3 -3.5 1.9 -4 -6 3 -0.3 1.1 3 6 -3 2.3 2.3 3 6 -3 3.2 2.1 -3 -6 3 5.4 2.4 -3 -6 3 4.6 2 -3 -6 3 6.9 0.9 2 6 -3 7.7 1.9 2 6 -3 7.3 2.3 -2 -6 3 8.8 2.3 -2 -6 3 7.9 1.9 1 6 -3 9.7 1.6 1 6 -3 8.1 2 -1 -6 3 7.7 1.8 -1 -6 3 10.5 2.2 -1 -6 3 9.6 1.2 -1 -6 3 13.6 1.9 0 6 -3 3.2 1.3 0 6 -3 3.2 1 0 6 -3 2.6 1.6 0 -6 3 2.7 1 0 -6 3 3.4 1.1 0 -6 3 2.1 1.2 0 -6 3 1.9 1.6 -1 6 -3 4.9 1 -1 6 -3 6.9 2 -1 6 -3 8.2 2 -1 6 -3 8.3 1.8 1 -6 3 3.2 1.3 1 -6 3 5.8 1.9 1 -6 3 5.1 0.7 -2 6 -3 12.5 1 -2 6 -3 18.7 2.8 -2 6 -3 13.7 1.1 -2 6 -3 14.4 2.4 -2 6 -3 15.8 2.6 2 -6 3 17.5 2.1 2 -6 3 16.4 2.9 -3 6 -3 11.3 2.5 3 -6 3 12.1 2.2 3 -6 3 10.9 2.4 -4 6 -3 0.2 2.4 4 -6 3 2.1 2.3 4 -6 3 -0.1 2 -5 6 -3 -1 1.1 -5 6 -3 -1.5 1 5 -6 3 1.1 2 5 -6 3 2 2.3 -6 6 -3 4.8 1.7 -6 6 -3 3.4 1.7 6 -6 3 -1.6 2.5 6 -6 3 4.8 2.5 -7 6 -3 6.2 2.2 -7 6 -3 6.3 2.4 7 -6 3 6.1 3.2 7 -6 3 -2.4 2.9 -8 6 -3 -3 2.8 -8 6 -3 -0.5 2.4 8 -6 3 1.5 3.6 8 -6 3 -1.5 3.1 -9 6 -3 10.8 3.4 -9 6 -3 17.5 4.2 9 -6 3 16 4.9 9 -6 3 21.7 5.4 -10 6 -3 7.2 5.4 -10 6 -3 8.8 4.1 10 -6 3 15.1 5.5 10 -6 3 10.6 5.3 -11 6 -3 4.4 5.9 -11 6 -3 0.1 4.7 11 -6 3 2.7 5.4 11 -6 3 4.1 9.8 -12 6 -3 13.6 8.2 -12 6 -3 2.3 5.7 12 -6 3 -1.8 5.9 -13 6 -3 4.9 10.3 -13 6 -3 6.9 11.3 13 -6 3 0.3 6.7 12 5 -3 5 11.1 12 5 -3 9.8 9.6 12 5 -3 -2.9 6.5 -12 -5 3 0.7 7.9 11 5 -3 -9.2 5.3 11 5 -3 7.6 9.5 11 5 -3 -0.4 11 -11 -5 3 -1.4 9.6 -11 -5 3 7.2 6.8 10 5 -3 30.8 7.7 10 5 -3 38.7 8 -10 -5 3 30.6 6.7 -10 -5 3 26.7 9 9 5 -3 13.2 5.6 9 5 -3 16.9 6.5 -9 -5 3 23 5.7 -9 -5 3 22.9 6.9 8 5 -3 144.39 9.7 8 5 -3 144.79 9.8 -8 -5 3 151.28 9.6 -8 -5 3 144.39 10.6 7 5 -3 8.3 4 7 5 -3 7.7 4.1 -7 -5 3 5.6 4.1 -7 -5 3 6.3 3.7 6 5 -3 26.6 4.8 6 5 -3 34.5 4.9 -6 -5 3 38.1 4.9 -6 -5 3 33 3.4 -6 -5 3 32 5 5 5 -3 205.58 9.3 5 5 -3 217.38 9.4 -5 -5 3 197.08 7.3 -5 -5 3 215.68 9.2 -5 -5 3 195.88 9.6 4 5 -3 25.4 3.4 4 5 -3 23.4 3.4 -4 -5 3 17.6 2.9 -4 -5 3 20.2 2 -4 -5 3 27.7 4 3 5 -3 31.9 3.2 3 5 -3 29 3.5 -3 -5 3 29.1 3.4 -3 -5 3 34.8 3.2 2 5 -3 1990.7 59.69 2 5 -3 1965.4 59.49 -2 -5 3 1998 59.79 -2 -5 3 1949.41 59.39 1 5 -3 2.5 1.3 1 5 -3 4 1.2 -1 -5 3 3.7 1.5 -1 -5 3 4 1.2 -1 -5 3 4.3 1.4 0 5 -3 138.49 5.3 0 5 -3 140.49 5.9 0 5 -3 143.49 5.2 0 -5 3 144.19 5.3 0 -5 3 138.29 5.9 0 -5 3 142.09 5.2 0 -5 3 138.39 5.2 -1 5 -3 1644.24 50.79 -1 5 -3 1724.83 52.09 -1 5 -3 1688.63 50.89 1 -5 3 1712.43 51.39 1 -5 3 1815.72 52.29 -2 5 -3 150.28 6.1 -2 5 -3 131.49 6 -2 5 -3 133.59 6 2 -5 3 144.99 6.4 2 -5 3 137.69 5.6 -3 5 -3 721.23 24.3 -3 5 -3 800.82 24.4 -3 5 -3 746.83 24.6 3 -5 3 795.42 24.6 3 -5 3 710.53 23.9 -4 5 -3 584.64 17.6 -4 5 -3 568.04 17.8 4 -5 3 602.24 19.8 4 -5 3 578.04 19.4 -5 5 -3 47.6 2.8 -5 5 -3 48.1 3.2 5 -5 3 50.19 4.4 5 -5 3 45 3.8 -6 5 -3 40.1 3.3 -6 5 -3 36.7 3.3 6 -5 3 38.4 4.6 6 -5 3 36.5 4.5 -7 5 -3 79.19 5.3 -7 5 -3 93.89 5.3 7 -5 3 86.59 5.9 7 -5 3 87.09 6.6 -8 5 -3 102.19 6.4 -8 5 -3 100.79 6.7 8 -5 3 107.89 7.8 8 -5 3 101.59 7.4 -9 5 -3 386.86 15.5 -9 5 -3 373.86 14.9 9 -5 3 403.46 16.9 9 -5 3 381.76 16.4 -10 5 -3 110.09 8.3 -10 5 -3 126.29 9.6 10 -5 3 119.79 9.5 10 -5 3 128.79 9.8 -11 5 -3 13.2 5.3 -11 5 -3 16.5 6.7 11 -5 3 10 6.1 11 -5 3 25.4 6.2 -12 5 -3 8.2 6.1 -12 5 -3 5.1 8.1 12 -5 3 -1.9 5.7 -13 5 -3 15.9 7.9 -13 5 -3 14.3 10.8 13 -5 3 2 7.2 12 4 -3 5.7 12.5 12 4 -3 0.9 6.2 12 4 -3 3.5 9.3 -12 -4 3 -14.3 7.3 11 4 -3 -1.8 7.2 11 4 -3 3.1 6 11 4 -3 -6.2 7.4 -11 -4 3 -0.9 6.4 -11 -4 3 3.6 9.2 10 4 -3 -14.7 5.6 10 4 -3 -10.6 5.8 -10 -4 3 -2.4 7.5 -10 -4 3 3.9 6.6 9 4 -3 28.2 6.4 9 4 -3 31.8 6.2 -9 -4 3 32.5 6.3 -9 -4 3 30.5 6.8 8 4 -3 21.7 4.8 8 4 -3 9.6 4.5 -8 -4 3 16.5 4.7 -8 -4 3 19.5 5.3 7 4 -3 -2.4 3.2 7 4 -3 2.6 3.7 -7 -4 3 2.3 3.1 -7 -4 3 2.2 3.6 6 4 -3 21.9 3.9 6 4 -3 18.3 3.9 -6 -4 3 19.1 3.6 -6 -4 3 17.4 3 -6 -4 3 23 4.1 5 4 -3 21.9 3.6 5 4 -3 19.2 3.4 -5 -4 3 22.4 3.4 -5 -4 3 21.6 3.5 -5 -4 3 22.1 2.5 4 4 -3 7.9 2.6 4 4 -3 5.2 2.1 -4 -4 3 6.7 1.5 -4 -4 3 2.9 2 -4 -4 3 4.7 2.4 3 4 -3 164.28 6.9 3 4 -3 155.58 6.5 -3 -4 3 158.08 6.6 -3 -4 3 153.88 6.8 2 4 -3 10.1 1.9 2 4 -3 10 1.7 -2 -4 3 10.4 2 -2 -4 3 6.4 1.5 1 4 -3 11.5 1.6 1 4 -3 11.8 1.4 -1 -4 3 10.1 1.7 -1 -4 3 11.5 1.6 -1 -4 3 11.8 1.5 0 4 -3 14.9 1.4 0 4 -3 14 1.5 0 4 -3 15.3 1.7 0 -4 3 14.3 1.5 0 -4 3 14 1.9 0 -4 3 14.8 1.4 -1 4 -3 8.8 1.7 -1 4 -3 6.7 0.9 -1 4 -3 6.4 0.8 1 -4 3 6.7 1.6 1 -4 3 5.9 1.3 -2 4 -3 0.9 0.4 -2 4 -3 0.4 0.4 -2 4 -3 -3.3 1.4 -2 4 -3 -1.6 1.3 -2 4 -3 -1.2 1.4 2 -4 3 -0.3 1.1 2 -4 3 1.3 1.2 -3 4 -3 196.48 7.5 -3 4 -3 154.08 5.7 -3 4 -3 178.08 7.2 -3 4 -3 173.18 5.7 3 -4 3 192.58 7.1 3 -4 3 181.18 7.3 -4 4 -3 42.6 4.1 -4 4 -3 32.7 2.2 4 -4 3 38.3 3.2 4 -4 3 30.5 3.4 -5 4 -3 103.59 4.6 -5 4 -3 97.19 4.8 5 -4 3 103.89 5.4 5 -4 3 93.99 5.7 -6 4 -3 2.3 2 -6 4 -3 3 2 6 -4 3 4.5 2.6 6 -4 3 5.2 2.6 -7 4 -3 7.4 2.6 -7 4 -3 7.6 2.7 7 -4 3 8 3.2 7 -4 3 10.8 3.2 -8 4 -3 9.3 3.3 -8 4 -3 5.4 3 8 -4 3 0.5 3.1 8 -4 3 2.2 3.4 -9 4 -3 4.7 4.3 9 -4 3 -4.4 3.8 9 -4 3 4 4.2 -10 4 -3 8.6 5.1 -10 4 -3 7 4.2 10 -4 3 -0.6 4.4 10 -4 3 2 4.5 -11 4 -3 -6 6.3 -11 4 -3 6.4 5.1 11 -4 3 2.4 5.3 11 -4 3 -1.2 4.6 -12 4 -3 8.5 8.2 -12 4 -3 3.8 6.2 12 -4 3 -5.2 5.6 -13 4 -3 10.6 7.7 -13 4 -3 3.3 11.3 13 -4 3 -3.2 6.3 13 3 -3 -3.7 6.9 13 3 -3 -22 8.6 -13 -3 3 12.7 9.2 12 3 -3 7.6 7.9 12 3 -3 3.4 7.6 12 3 -3 3.8 6.4 -12 -3 3 0.4 7.1 11 3 -3 -5.6 5.4 11 3 -3 6.5 7 11 3 -3 -4 6.3 -11 -3 3 -3.6 5.6 -11 -3 3 -1.6 8 10 3 -3 17 6 10 3 -3 32.6 6.6 10 3 -3 19.1 6.4 -10 -3 3 11.6 7.5 -10 -3 3 22.7 6.1 9 3 -3 441.86 18.1 9 3 -3 426.56 17 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657.33 20.4 -4 3 -3 678.73 21.4 -4 3 -3 641.84 20.5 4 -3 3 635.64 21.1 4 -3 3 645.34 21.3 -5 3 -3 897.51 29.2 -5 3 -3 1062.99 31.6 -5 3 -3 914.61 29.1 5 -3 3 944.51 30.1 5 -3 3 928.41 29.9 5 -3 3 883.91 27.7 -6 3 -3 279.07 10.7 -6 3 -3 283.87 10.7 6 -3 3 291.07 11.5 6 -3 3 285.97 11.3 6 -3 3 274.97 9 -7 3 -3 12.7 3.1 -7 3 -3 8.6 3 7 -3 3 7.7 2.3 7 -3 3 8.1 3.1 7 -3 3 10.3 3.5 7 -3 3 9.8 1.5 -8 3 -3 2.8 3.4 -8 3 -3 3.4 3 8 -3 3 -0.5 3 8 -3 3 0.2 3.3 -9 3 -3 90.09 11.5 9 -3 3 109.39 8.3 9 -3 3 108.49 8 -10 3 -3 34.8 5.6 -10 3 -3 34.1 6.6 10 -3 3 32.3 6.2 -11 3 -3 9.4 5.6 -11 3 -3 9.1 7 11 -3 3 9.5 5.2 11 -3 3 11.4 5.9 -12 3 -3 8.9 9.1 -12 3 -3 7.8 6.8 -13 3 -3 4.3 7.7 13 -3 3 9.5 7.2 13 2 -3 -4 6.4 13 2 -3 3.2 7.6 -13 -2 3 -2.4 8.3 12 2 -3 1.3 6.6 12 2 -3 4.8 7.3 12 2 -3 -6.5 6.6 -12 -2 3 11.6 12 -12 -2 3 -3.1 6.6 11 2 -3 8.3 5.8 11 2 -3 2.8 5.9 -11 -2 3 -2.9 7.5 -11 -2 3 2.9 6 10 2 -3 0.6 5.2 10 2 -3 0 5.1 10 2 -3 -2.6 4.7 -10 -2 3 1.9 6.3 -10 -2 3 3.2 5.1 9 2 -3 8.9 4.3 9 2 -3 1.2 4.2 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109.69 2 -1 3 3822.22 109.49 2 -1 3 3747.23 109.89 2 -1 3 3659.03 109.59 -3 1 -3 22.9 2.5 -3 1 -3 27.3 2.7 -3 1 -3 24.8 2.3 -3 1 -3 22.4 2.3 3 -1 3 21 2.3 3 -1 3 25.1 2.3 3 -1 3 29.2 2.3 3 -1 3 21.1 2.1 -4 1 -3 2510.95 73.89 -4 1 -3 2386.76 73.79 -4 1 -3 2535.25 74.09 4 -1 3 2456.55 73.19 4 -1 3 2493.35 73.59 4 -1 3 2438.96 73.79 4 -1 3 2407.06 73.59 -5 1 -3 377.76 13.7 -5 1 -3 383.86 13.7 5 -1 3 377.36 12.9 5 -1 3 376.26 13.5 5 -1 3 388.56 13.5 5 -1 3 386.86 13.4 -6 1 -3 0.4 2.4 -6 1 -3 3.7 2.4 6 -1 3 -0.3 2.1 6 -1 3 1.5 2.3 6 -1 3 4.3 2.2 6 -1 3 10.5 2.3 -7 1 -3 3.3 3.1 -7 1 -3 10.4 3.2 7 -1 3 8.9 3.4 7 -1 3 8.6 2.9 7 -1 3 3.2 2.5 7 -1 3 11.2 3 -8 1 -3 5.9 3.9 8 -1 3 -1.4 2.7 8 -1 3 1.3 3 8 -1 3 3.4 3.1 8 -1 3 3.2 3.3 -9 1 -3 182.18 10.3 -9 1 -3 171.88 11.3 9 -1 3 169.28 8.3 9 -1 3 188.88 9.7 9 -1 3 162.08 9.7 9 -1 3 172.58 9.1 -10 1 -3 19.2 6.8 -10 1 -3 14.8 5.1 10 -1 3 16.2 4 10 -1 3 11.8 4.2 10 -1 3 14 4.9 10 -1 3 15.8 4.9 -11 1 -3 -1.9 7.8 -11 1 -3 -1.4 5.6 11 -1 3 2.8 3.7 11 -1 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-4 -4 84.79 4.9 -3 4 4 82.39 3.9 -3 4 4 86.19 3.7 -3 4 4 84.29 3.7 2 -4 -4 1966.9 59.39 2 -4 -4 1976.9 59.89 2 -4 -4 2140.19 60.89 2 -4 -4 1974.7 60.09 -2 4 4 2033.3 59.89 -2 4 4 2007.2 59.99 -2 4 4 1953.1 59.59 1 -4 -4 5299.17 152.28 1 -4 -4 4921.31 151.98 -1 4 4 5020.1 152.18 -1 4 4 5399.86 152.38 0 -4 -4 32.8 3 0 -4 -4 34.9 2.6 0 -4 -4 38 2.2 0 4 4 31.3 2.7 0 4 4 37.1 2.4 0 4 4 38.1 3.1 -1 -4 -4 3.3 1.5 -1 -4 -4 5 2 1 4 4 2.3 2.1 1 4 4 3.3 1 1 4 4 2.6 1.6 -2 -4 -4 119.99 6.4 -2 -4 -4 141.99 6.4 2 4 4 125.69 6.4 2 4 4 138.69 6.6 2 4 4 139.69 4.5 -3 -4 -4 8 2.5 -3 -4 -4 9.9 2.9 3 4 4 6.5 2.6 3 4 4 8.6 1.7 3 4 4 9 2.7 -4 -4 -4 758.52 25.7 -4 -4 -4 726.03 25.9 4 4 4 769.92 25.8 4 4 4 777.12 23.9 4 4 4 796.42 26.1 -5 -4 -4 215.78 10 -5 -4 -4 211.68 10.6 5 4 4 196.98 9.7 5 4 4 221.58 10.5 5 4 4 213.78 8.1 -6 -4 -4 74.19 8.5 6 4 4 70.19 4.5 6 4 4 71.19 7 6 4 4 77.99 4.4 6 4 4 59.49 6.2 -7 -4 -4 78.99 7.7 -7 -4 -4 71.59 8.4 7 4 4 80.69 7.5 7 4 4 78.49 5.5 7 4 4 72.59 4.9 7 4 4 87.49 8.3 -8 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7.8 7.4 9 5 4 10.7 6 9 5 4 7.1 4 9 5 4 1.7 6.7 -10 -5 -4 -6 9.2 -10 -5 -4 11.4 7 10 5 4 -6 7.8 10 5 4 -4 6.6 10 5 4 5.2 4.5 -11 -5 -4 0.3 7.7 11 5 4 3.9 5.1 11 5 4 -10.5 8.3 -12 -5 -4 10.3 9.6 12 5 4 13.4 11 12 5 4 3.9 7.8 12 5 4 1.4 12.7 13 -6 -4 7 7.1 -13 6 4 -9.3 6.4 -13 6 4 19 9.8 12 -6 -4 -1.6 6.2 -12 6 4 -10.6 7 -12 6 4 7.9 5.5 11 -6 -4 130.99 11.7 -11 6 4 123.89 10.8 -11 6 4 152.28 9.5 10 -6 -4 18.7 10.1 -10 6 4 10 5.1 -10 6 4 17.1 4.1 9 -6 -4 8 4.8 -9 6 4 9 4.2 -9 6 4 11.4 3.3 8 -6 -4 551.94 22.2 -8 6 4 570.94 18.9 -8 6 4 572.44 19.2 7 -6 -4 -5.9 3.4 -7 6 4 0.6 2.9 -7 6 4 1.4 1.8 -7 6 4 -4 2.2 6 -6 -4 50.19 5.7 -6 6 4 48.9 3.2 -6 6 4 55.79 3.6 -6 6 4 51.79 4.3 5 -6 -4 -1 2.5 -5 6 4 -0.6 1.7 -5 6 4 2 1.3 -5 6 4 1.8 1.4 4 -6 -4 2.8 2.2 -4 6 4 7.8 1.9 -4 6 4 7.2 1.4 -4 6 4 10.6 1.7 3 -6 -4 1081.99 33.3 3 -6 -4 1029.3 32 -3 6 4 1032.1 31.6 -3 6 4 1027.7 31.5 -3 6 4 998.1 31.7 2 -6 -4 324.27 10.5 2 -6 -4 320.57 11.3 2 -6 -4 341.47 12.2 -2 6 4 334.37 11.3 -2 6 4 337.57 12.3 -2 6 4 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2.4 3.4 9 -9 6 3.3 4.7 9 -9 6 4 5 -10 9 -6 -0.1 4.9 -10 9 -6 2.5 4 -10 9 -6 -3.5 8.8 10 -9 6 7.4 5.7 10 -9 6 -5.4 5.2 -11 9 -6 -12.3 10.9 -11 9 -6 4.5 7 -11 9 -6 1.4 4.7 11 -9 6 -4 5.7 11 -9 6 -1.8 5.6 -12 9 -6 2.2 6 -12 9 -6 8.8 10.2 12 -9 6 -2.9 6.7 12 -9 6 -4.3 6.5 12 8 -6 13.2 11.6 -12 -8 6 5.3 9 11 8 -6 15.7 9.7 11 8 -6 -4.7 9.5 -11 -8 6 -1.6 7.1 10 8 -6 -3.9 7.6 10 8 -6 0.3 8.2 -10 -8 6 17 9.6 -10 -8 6 4.4 6.8 9 8 -6 1.7 8.8 -9 -8 6 -3.4 9.9 -9 -8 6 3.9 5.7 8 8 -6 117.79 10.6 8 8 -6 133.09 10.6 -8 -8 6 117.59 9.7 -8 -8 6 116.19 7.2 7 8 -6 15.2 5.1 7 8 -6 10.9 5.8 -7 -8 6 13.4 5 -7 -8 6 11.7 3.1 6 8 -6 91.59 7.9 6 8 -6 94.59 7.7 -6 -8 6 99.49 7.4 -6 -8 6 84.79 4.6 -6 -8 6 79.79 8.3 5 8 -6 32.2 5.2 -5 -8 6 30.2 2.8 -5 -8 6 46.5 6 -5 -8 6 34.9 4.7 4 8 -6 65.79 5.9 4 8 -6 73.79 5.4 -4 -8 6 60.09 5.3 -4 -8 6 69.19 6.1 3 8 -6 97.19 5.8 3 8 -6 96.79 6.3 -3 -8 6 96.49 6 -3 -8 6 112.29 6.8 -3 -8 6 103.79 6.6 2 8 -6 2032.1 61.99 2 8 -6 2027.6 61.79 -2 -8 6 1971.2 61.69 -2 -8 6 2018.5 62.59 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3.3 -6 5 -6 17.7 3.2 6 -5 6 12.2 3.3 6 -5 6 14.1 3.6 -7 5 -6 1.6 2.9 -7 5 -6 0.4 2.8 7 -5 6 1.2 3.2 7 -5 6 -3.4 2.9 -8 5 -6 70.39 6.8 -8 5 -6 68.49 6.3 8 -5 6 61.39 6.7 8 -5 6 66.99 6.8 -9 5 -6 21.8 4.7 -9 5 -6 25.4 5.6 9 -5 6 26.7 5.3 -10 5 -6 5.9 4.5 -10 5 -6 3.5 5.6 10 -5 6 -3.1 4.4 10 -5 6 4.8 4.9 -11 5 -6 4.2 7.2 11 -5 6 0.9 5.4 11 -5 6 9.5 5.8 -12 5 -6 9.6 9.3 -12 5 -6 11.2 6.8 12 -5 6 2.2 6.6 12 -5 6 9.6 6.8 13 4 -6 18 10.7 12 4 -6 -4.6 5.9 12 4 -6 18.7 16.3 12 4 -6 4.9 10.4 -12 -4 6 -18.5 7 11 4 -6 3.6 7.1 11 4 -6 -1.7 7 -11 -4 6 6.5 6.2 -11 -4 6 -1.6 8.8 10 4 -6 -6.9 5.4 10 4 -6 -3.5 6 -10 -4 6 15.3 7.1 -10 -4 6 -9.6 8.7 9 4 -6 128.29 9.8 9 4 -6 129.89 9.9 -9 -4 6 130.99 9.5 -9 -4 6 122.29 11.2 8 4 -6 27.4 5.4 -8 -4 6 28.8 5 -8 -4 6 33.5 6.2 7 4 -6 14.6 3.9 7 4 -6 16.3 4.2 -7 -4 6 14.7 4.5 -7 -4 6 19.1 4.3 6 4 -6 190.98 9.3 6 4 -6 210.78 9.5 -6 -4 6 195.48 9.9 -6 -4 6 202.88 9.3 5 4 -6 180.98 8.1 5 4 -6 186.98 8.4 -5 -4 6 173.88 8.4 -5 -4 6 166.48 8 4 4 -6 14.6 3 4 4 -6 16.7 2.7 -4 -4 6 23.2 3.4 -4 -4 6 16.5 2.8 3 4 -6 27.5 3.3 3 4 -6 21.8 2.8 -3 -4 6 26.2 3.1 -3 -4 6 28.4 3 2 4 -6 0.2 1.2 2 4 -6 -1.1 1.4 -2 -4 6 -0.4 1.2 -2 -4 6 -1 1.4 -2 -4 6 1.2 1.4 1 4 -6 122.89 5.3 1 4 -6 124.99 5.2 1 4 -6 123.09 5.2 -1 -4 6 123.39 5.1 -1 -4 6 126.49 5.4 -1 -4 6 119.39 5.3 0 4 -6 865.51 26.9 0 4 -6 866.91 27.2 0 4 -6 865.51 26.6 0 -4 6 867.01 26.5 0 -4 6 865.61 26.9 0 -4 6 864.61 27.2 -1 4 -6 406.76 14.3 -1 4 -6 428.36 13.8 -1 4 -6 418.06 13.4 1 -4 6 421.66 13.2 -2 4 -6 52.29 3.2 -2 4 -6 48.9 3.9 -2 4 -6 49 3.7 -2 4 -6 49.8 3 2 -4 6 47.7 3.4 2 -4 6 50.59 2.2 -3 4 -6 112.09 5 -3 4 -6 112.09 5.7 -3 4 -6 107.99 5 3 -4 6 116.89 3.8 3 -4 6 106.49 5.5 -4 4 -6 0.7 1.7 -4 4 -6 0.6 2 -4 4 -6 3.7 2.6 4 -4 6 1.7 2 -5 4 -6 55.29 4.1 -5 4 -6 47.1 4.1 5 -4 6 52.89 4.4 5 -4 6 43 4.3 -6 4 -6 152.38 7.6 -6 4 -6 160.28 7.8 6 -4 6 165.48 8.1 6 -4 6 165.48 8.1 -7 4 -6 52.49 5.3 -7 4 -6 52.19 5.5 7 -4 6 43.5 5.1 7 -4 6 43.6 5.3 -8 4 -6 176.28 9.2 -8 4 -6 185.88 10 8 -4 6 177.78 9.7 8 -4 6 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6 1.6 1.3 1 3 -6 3.7 1.2 1 3 -6 1.9 1.3 1 3 -6 1.9 1 -1 -3 6 3 1.2 -1 -3 6 3 1.2 -1 -3 6 0.9 1.2 0 3 -6 2 1.1 0 3 -6 3.8 1.3 0 3 -6 2.4 1.1 0 -3 6 2.7 1 0 -3 6 5.6 1.5 0 -3 6 4.1 1.4 -1 3 -6 3.7 1.3 -1 3 -6 3.4 1.5 -1 3 -6 4.9 1.4 1 -3 6 1.9 1.4 1 -3 6 3 1 -2 3 -6 0.9 1.6 -2 3 -6 0.2 1.5 -2 3 -6 -0.6 1.2 2 -3 6 0.7 1.1 2 -3 6 -0.1 0.9 -3 3 -6 178.28 7.3 -3 3 -6 186.88 7.5 -3 3 -6 176.18 7.3 3 -3 6 204.28 6.7 3 -3 6 203.28 7.9 3 -3 6 168.68 6.5 -4 3 -6 -1.7 1.6 -4 3 -6 -1.4 2.1 -4 3 -6 -2.8 2 4 -3 6 -1.4 1.9 4 -3 6 0.3 1.1 4 -3 6 -1.5 1.1 -5 3 -6 68.89 4.8 -5 3 -6 68.19 4.7 -5 3 -6 47.9 5.2 5 -3 6 63.19 4.4 5 -3 6 60.89 4.7 5 -3 6 63.59 3.3 5 -3 6 56.59 3.5 -6 3 -6 21 3.5 -6 3 -6 20.1 3.5 6 -3 6 16.5 2.2 6 -3 6 22.2 2.3 6 -3 6 20.8 3.6 6 -3 6 12.9 3.1 -7 3 -6 4.5 3.1 -7 3 -6 5.7 3.6 7 -3 6 6.1 3.3 7 -3 6 5.4 2 7 -3 6 1.9 1.7 7 -3 6 -0.2 2.8 -8 3 -6 -3.7 3.3 -8 3 -6 -1.5 4.2 8 -3 6 -0.7 3.8 8 -3 6 2.4 1.9 8 -3 6 2.3 1.9 8 -3 6 0.3 3.4 -9 3 -6 3.1 4.3 -9 3 -6 6 5.1 9 -3 6 4.2 4 9 -3 6 3.7 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30 17.9 13.1 2 3 -30 6.3 7.6 2 3 -30 -5.8 11.7 -2 -3 30 3.7 11.9 1 3 -30 -4.3 12.1 1 3 -30 7.6 8.3 -1 -3 30 26.3 12.1 0 3 -30 9.3 12.4 0 -3 30 13.4 13.2 -1 3 -30 3 11.5 -1 3 -30 0.8 12.3 1 -3 30 8.7 12.5 -2 3 -30 -2.5 13.5 -2 3 -30 -8.2 13.3 6 2 -30 -11.7 12.9 -6 -2 30 14.2 13.7 5 2 -30 16.2 12.8 -5 -2 30 4.2 12.8 4 2 -30 19.3 12.1 -4 -2 30 -15.6 11.8 3 2 -30 17 11.6 3 2 -30 -0.5 6.5 -3 -2 30 16.3 12.7 2 2 -30 38.4 12.7 2 2 -30 21 7.6 -2 -2 30 23.3 12.4 1 2 -30 8.7 8 1 2 -30 -20.9 10.7 -1 -2 30 26 12.9 0 2 -30 31.5 9.9 0 2 -30 9.9 12 0 -2 30 13.9 12.4 -1 2 -30 23.7 12.1 -1 2 -30 31.6 13 1 -2 30 -2.5 12.6 -2 2 -30 26.9 14 -2 2 -30 -0.8 13.7 6 1 -30 0.2 13.1 -6 -1 30 -16.2 13.9 5 1 -30 12.9 12.2 -5 -1 30 11.9 12.9 4 1 -30 15.9 12.6 -4 -1 30 8.7 12.6 3 1 -30 -0.6 11.9 3 1 -30 -1.9 6.8 -3 -1 30 -9.3 12.5 2 1 -30 -1.6 6.4 2 1 -30 29.4 12.5 -2 -1 30 -16.7 11.7 1 1 -30 9.8 7.9 1 1 -30 -7.8 11.4 -1 -1 30 0.9 12.5 0 1 -30 4.5 9.5 0 1 -30 4.5 12.4 0 -1 30 -8.1 12.7 -1 1 -30 -18.6 12.4 -1 1 -30 -14.3 11.4 1 -1 30 -27 12.2 6 0 -30 24.4 13.5 -6 0 30 1.3 13.6 5 0 -30 -2.9 12.3 -5 0 30 8.9 12.4 4 0 -30 13.9 12.9 -4 0 30 6.6 11.6 3 0 -30 20.5 12.5 -3 0 30 -2.3 12.3 2 0 -30 7.6 6.4 2 0 -30 -2.9 11.3 -2 0 30 13.5 12.6 1 0 -30 12.2 8.1 1 0 -30 11.2 12.2 -1 0 30 11.1 12.8 0 0 -30 37.2 11.1 0 0 -30 14.6 12.5 0 0 30 49.6 14.1 -1 0 -30 6.7 11.6 -1 0 -30 21.3 13.5 1 0 30 -2.7 12.6 6 -1 -30 10.5 13 5 -1 -30 -12.6 12.1 -5 1 30 4.2 12.2 4 -1 -30 48.5 13.6 -4 1 30 -1.9 11.1 3 -1 -30 10.4 12.4 -3 1 30 0.1 11.8 2 -1 -30 -1.3 11.3 2 -1 -30 -3.2 8.8 -2 1 30 4 11.7 1 -1 -30 3.4 8.2 1 -1 -30 3 11.4 -1 1 30 -22.6 12.4 0 -1 -30 9.4 13.2 0 -1 -30 -23.9 10 0 1 30 -8.4 12.2 -1 -1 -30 22.5 13.1 -1 -1 -30 14.3 12.2 1 1 30 29.3 14 5 -2 -30 31 13.2 -5 2 30 2 13.8 4 -2 -30 12 12.9 -4 2 30 5.2 12.2 3 -2 -30 4.7 12.3 -3 2 30 32.1 13.1 2 -2 -30 13.8 11.7 -2 2 30 -4.8 11.8 1 -2 -30 14.1 12.6 -1 2 30 5.4 13.8 0 -2 -30 17.1 12.6 0 -2 -30 -2.4 12 0 2 30 16.6 13.4 5 -3 -30 -2.2 13 -5 3 30 2.5 12.9 4 -3 -30 -11 12.2 -4 3 30 11 13.2 3 -3 -30 9.8 12.4 -3 3 30 18.9 13.1 2 -3 -30 0.4 11.8 -2 3 30 21.5 14.1 1 -3 -30 1 12.4 -1 3 30 -3.1 14.4 0 -3 -30 13.2 13.1 4 -4 -30 16.5 12.9 -4 4 30 -20.7 12.1 3 -4 -30 21 12.6 -3 4 30 8.1 13.7 2 -4 -30 -10.8 11.7 -2 4 30 -5.9 13.5 1 -4 -30 14.5 13.4 1 -4 -30 3.4 12.5 3 -5 -30 2.9 7.6 3 -5 -30 -31.5 12.2 2 -5 -30 30.1 13.4 2 7 -31 -11.7 12.8 3 6 -31 -26.3 12.7 2 6 -31 12.7 13.5 -2 -6 31 -13 13.5 1 6 -31 4 12.9 -1 -6 31 -23.3 13 4 5 -31 -19.1 13.5 3 5 -31 -4.2 12.5 -3 -5 31 16.4 14.1 2 5 -31 -22.7 12.7 -2 -5 31 10.4 13.1 1 5 -31 5.9 12.7 -1 -5 31 -6.4 13.2 0 5 -31 29.6 15.1 0 5 -31 -5.5 10.6 4 4 -31 13.2 13 -4 -4 31 21.9 14.5 3 4 -31 20.2 13.2 -3 -4 31 24.8 13.6 2 4 -31 20.5 14 -2 -4 31 -6.2 13.1 1 4 -31 14.9 10.2 1 4 -31 45.7 13.7 -1 -4 31 3.2 13.5 0 4 -31 33.5 15 0 4 -31 -1.4 10.4 0 -4 31 -26.2 14 4 3 -31 3.2 13.5 -4 -3 31 33.7 13.9 3 3 -31 -8.1 12.5 -3 -3 31 -0.5 13.6 2 3 -31 17.6 13.3 -2 -3 31 6.7 14 1 3 -31 -7.4 12.6 1 3 -31 10.6 11.4 -1 -3 31 41.2 14.5 0 3 -31 -0.5 13.1 0 -3 31 16.4 14.4 4 2 -31 -20.5 13.6 -4 -2 31 10.1 14 3 2 -31 23.1 14.3 -3 -2 31 15.6 13.8 2 2 -31 13.5 13 -2 -2 31 -7.4 13.1 1 2 -31 4.7 12.9 -1 -2 31 -0.5 12.9 0 2 -31 -7.7 12.7 0 -2 31 -1.6 13.9 4 1 -31 -7.6 13.1 -4 -1 31 -21.9 12.9 3 1 -31 -4.1 12.4 -3 -1 31 -20.9 12.4 2 1 -31 1.5 13.4 -2 -1 31 -0.9 15.3 1 1 -31 24.2 13.6 -1 -1 31 20.6 14.7 0 1 -31 29.2 14.2 4 0 -31 0.2 14.1 -4 0 31 2.3 12.6 3 0 -31 -11.6 12.9 -3 0 31 5.2 13.4 2 0 -31 22.4 13.4 -2 0 31 -0.4 12.5 1 0 -31 6.9 12.6 -1 0 31 16.5 15.1 4 -1 -31 14.6 13.9 3 -1 -31 19.3 14 -3 1 31 10.5 14.3 2 -1 -31 26.1 13.3 -2 1 31 31.4 13.7 1 -1 -31 19.2 12.9 3 -2 -31 6.2 13.5 2 -2 -31 -7.7 12.6 _iucr_refine_instructions_details ; 01.res created by SHELXL-2014/7 TITL 01_a.res in P-1 REM Old TITL 01 in P-1 REM SHELXT solution in P-1 REM R1 0.236, Rweak 0.023, Alpha 0.083, Orientation as input REM Formula found by SHELXT: C99 N8 O2 F14 CELL 0.71073 10.3304 17.8901 23.7841 96.034 99.172 99.186 ZERR 2 0.0012 0.002 0.0031 0.005 0.005 0.005 LATT 1 SFAC C H F N O UNIT 200 156 24 16 10 SIMU 0.01 0.01 2 O5 > C100 SIMU 0.01 0.02 2 C18 C19 C20 H20 C21 C22 H22 C23 C24 H24a H24b H24c H97a L.S. 30 PLAN 20 SIZE 0.14 0.17 0.25 TEMP 17.85 list 4 fmap 2 acta REM REM REM WGHT 0.079900 1.301600 FVAR 0.40389 F1 3 0.782548 1.105783 0.757864 11.00000 0.05712 0.09376 = 0.08440 0.00654 0.02118 0.02585 F2 3 0.768135 1.076350 0.667080 11.00000 0.04734 0.09753 = 0.06904 0.02373 -0.01303 0.01301 F3 3 0.778919 0.990456 0.723181 11.00000 0.04666 0.06894 = 0.09991 0.02233 -0.00057 -0.00310 O1 5 1.019957 1.056641 0.780303 11.00000 0.03756 0.05185 = 0.04013 0.00968 -0.00246 0.00428 N1 4 1.204875 1.153653 0.785785 11.00000 0.03938 0.04423 = 0.03513 0.00230 0.00227 0.00617 N2 4 1.013589 1.159757 0.721676 11.00000 0.05078 0.04232 = 0.04151 0.00778 -0.00059 0.01124 C1 1 1.126106 1.191313 0.750934 11.00000 0.05229 0.03769 = 0.04342 0.00704 0.00593 0.01268 AFIX 43 H1 2 1.156790 1.242495 0.748674 11.00000 -1.20000 AFIX 0 C2 1 1.148590 1.085791 0.803275 11.00000 0.03927 0.04088 = 0.03215 0.00246 0.00653 0.00968 C3 1 1.234193 1.062886 0.844697 11.00000 0.03758 0.04845 = 0.03047 -0.00015 0.00873 0.01378 C4 1 1.353930 1.121676 0.855215 11.00000 0.03638 0.05065 = 0.03445 -0.00772 0.00634 0.01344 C5 1 1.333543 1.177117 0.818407 11.00000 0.03923 0.04746 = 0.03951 -0.00522 0.00872 0.01006 C6 1 1.428797 1.239995 0.816334 11.00000 0.05100 0.05145 = 0.06070 -0.00456 0.01584 0.00372 AFIX 43 H6 2 1.412946 1.275067 0.790983 11.00000 -1.20000 AFIX 0 C7 1 1.548645 1.248279 0.853694 11.00000 0.04351 0.06379 = 0.08579 -0.01935 0.00858 -0.00248 AFIX 43 H7 2 1.615421 1.289772 0.853527 11.00000 -1.20000 AFIX 0 C8 1 1.571143 1.195674 0.891524 11.00000 0.04037 0.07689 = 0.07521 -0.02330 -0.00880 0.01202 AFIX 43 H8 2 1.652573 1.202954 0.916405 11.00000 -1.20000 AFIX 0 C9 1 1.475729 1.132998 0.893060 11.00000 0.04489 0.06187 = 0.05074 -0.00682 0.00013 0.01754 AFIX 43 H9 2 1.492141 1.098653 0.918948 11.00000 -1.20000 AFIX 0 C10 1 1.208803 0.993214 0.872063 11.00000 0.04578 0.04930 = 0.03263 0.00154 0.00743 0.01659 C11 1 1.310403 0.953705 0.889719 11.00000 0.05366 0.06831 = 0.05113 0.00812 0.00748 0.02484 AFIX 43 H11 2 1.395980 0.970709 0.883262 11.00000 -1.20000 AFIX 0 C12 1 1.285698 0.889357 0.916796 11.00000 0.08967 0.06661 = 0.07133 0.01923 0.00947 0.03907 AFIX 43 H12 2 1.355021 0.863883 0.928455 11.00000 -1.20000 AFIX 0 C13 1 1.160709 0.862797 0.926607 11.00000 0.08410 0.05800 = 0.07503 0.02328 0.02182 0.01771 AFIX 43 H13 2 1.145449 0.820252 0.945600 11.00000 -1.20000 AFIX 0 C14 1 1.058085 0.899483 0.908180 11.00000 0.06457 0.05976 = 0.06798 0.01447 0.02169 0.01069 AFIX 43 H14 2 0.972416 0.880796 0.913761 11.00000 -1.20000 AFIX 0 C15 1 1.081057 0.964168 0.881315 11.00000 0.05150 0.05456 = 0.04629 0.00494 0.00579 0.01466 AFIX 43 H15 2 1.010587 0.988616 0.869266 11.00000 -1.20000 AFIX 0 C16 1 0.977094 1.078754 0.723889 11.00000 0.04246 0.04238 = 0.03642 0.00871 -0.00324 0.00768 C17 1 0.825550 1.062181 0.718202 11.00000 0.04596 0.05384 = 0.05657 0.01262 0.00013 0.01288 C18 1 1.024131 1.030737 0.677561 11.00000 0.03641 0.04730 = 0.04368 -0.00060 -0.00519 0.00861 C19 1 1.030457 0.954818 0.682417 11.00000 0.05947 0.05284 = 0.06503 -0.00450 -0.00064 0.00989 AFIX 43 H19 2 1.010162 0.934057 0.714875 11.00000 -1.20000 AFIX 0 C20 1 1.067542 0.909677 0.638205 11.00000 0.06156 0.06204 = 0.09722 -0.02213 -0.01120 0.02186 AFIX 43 H20 2 1.072598 0.858950 0.641952 11.00000 -1.20000 AFIX 0 C21 1 1.096826 0.938265 0.589206 11.00000 0.04712 0.09905 = 0.07080 -0.03027 -0.00403 0.02110 C22 1 1.092116 1.013355 0.585472 11.00000 0.06325 0.10399 = 0.06049 -0.00897 0.00829 0.01865 AFIX 43 H22 2 1.113882 1.034094 0.553218 11.00000 -1.20000 AFIX 0 C23 1 1.055632 1.059509 0.628642 11.00000 0.05566 0.06989 = 0.05043 -0.00034 0.00419 0.01434 AFIX 43 H23 2 1.052279 1.110371 0.624699 11.00000 -1.20000 AFIX 0 C24 1 1.131274 0.886344 0.541570 11.00000 0.08334 0.15882 = 0.12059 -0.07198 0.00788 0.04147 AFIX 137 H24A 2 1.189957 0.915819 0.521331 11.00000 -1.50000 H24B 2 1.051186 0.862421 0.515411 11.00000 -1.50000 H24C 2 1.174550 0.847824 0.557721 11.00000 -1.50000 AFIX 0 F4 3 0.763349 0.929738 0.553878 11.00000 0.05008 0.05677 = 0.09686 0.00093 0.01109 -0.01670 F5 3 0.750555 0.821986 0.503049 11.00000 0.05521 0.09362 = 0.09460 -0.01625 0.03110 0.00576 F6 3 0.752330 0.826965 0.593225 11.00000 0.04262 0.08210 = 0.08386 0.01846 -0.00531 0.00643 O2 5 0.510926 0.766035 0.533747 11.00000 0.03550 0.03173 = 0.04586 0.00514 0.00206 0.00089 N3 4 0.329839 0.780203 0.465738 11.00000 0.04041 0.03314 = 0.03429 0.00704 0.00471 0.00431 N4 4 0.515704 0.877255 0.482933 11.00000 0.05389 0.03878 = 0.03918 0.00632 0.00681 -0.00224 C25 1 0.406292 0.843432 0.452163 11.00000 0.05476 0.03600 = 0.03426 0.00786 0.00898 0.00677 AFIX 43 H25 2 0.376167 0.862513 0.418539 11.00000 -1.20000 AFIX 0 C26 1 0.380371 0.742945 0.510211 11.00000 0.03551 0.02805 = 0.03284 0.00136 0.00346 0.00638 C27 1 0.288740 0.684479 0.519723 11.00000 0.03427 0.03062 = 0.03208 0.00419 0.00654 0.00778 C28 1 0.170938 0.683110 0.476315 11.00000 0.03580 0.03579 = 0.03300 0.00266 0.00683 0.01014 C29 1 0.046330 0.635357 0.460960 11.00000 0.03581 0.04599 = 0.04484 0.00648 0.00475 0.00329 AFIX 43 H29 2 0.024800 0.594164 0.480636 11.00000 -1.20000 AFIX 0 C30 1 -0.044072 0.650251 0.416243 11.00000 0.03570 0.06158 = 0.05687 0.00329 -0.00221 0.00186 AFIX 43 H30 2 -0.127491 0.618981 0.406247 11.00000 -1.20000 AFIX 0 C31 1 -0.013843 0.710642 0.385786 11.00000 0.04705 0.06428 = 0.04227 0.00883 -0.00633 0.01190 AFIX 43 H31 2 -0.077334 0.719274 0.355940 11.00000 -1.20000 AFIX 0 C32 1 0.107974 0.757827 0.398907 11.00000 0.04937 0.05084 = 0.03284 0.00884 0.00227 0.01247 AFIX 43 H32 2 0.128616 0.798445 0.378565 11.00000 -1.20000 AFIX 0 C33 1 0.198677 0.742797 0.443377 11.00000 0.03673 0.03576 = 0.03134 0.00178 0.00577 0.00797 C34 1 0.306592 0.634662 0.564826 11.00000 0.03790 0.02882 = 0.03389 0.00315 0.00583 0.00485 C35 1 0.430471 0.616816 0.584459 11.00000 0.03716 0.04802 = 0.04682 0.01081 0.01054 0.00896 AFIX 43 H35 2 0.503769 0.636627 0.568989 11.00000 -1.20000 AFIX 0 C36 1 0.445956 0.569861 0.626804 11.00000 0.04826 0.06321 = 0.05891 0.02384 0.00714 0.02164 AFIX 43 H36 2 0.529737 0.559008 0.639973 11.00000 -1.20000 AFIX 0 C37 1 0.338205 0.539128 0.649548 11.00000 0.06561 0.06776 = 0.06327 0.03756 0.01574 0.01565 AFIX 43 H37 2 0.348959 0.506953 0.677558 11.00000 -1.20000 AFIX 0 C38 1 0.214286 0.556082 0.630771 11.00000 0.05464 0.07836 = 0.06119 0.03266 0.01923 0.00697 AFIX 43 H38 2 0.141194 0.535319 0.645988 11.00000 -1.20000 AFIX 0 C39 1 0.199189 0.604064 0.589243 11.00000 0.04037 0.06315 = 0.04994 0.01799 0.01121 0.01196 AFIX 43 H39 2 0.115775 0.616207 0.577328 11.00000 -1.20000 AFIX 0 C40 1 0.554144 0.848128 0.536315 11.00000 0.03942 0.03294 = 0.04050 0.00396 0.00804 -0.00088 C41 1 0.706867 0.856692 0.546730 11.00000 0.04655 0.04683 = 0.06402 0.00046 0.01280 -0.00110 C42 1 0.508881 0.890207 0.586406 11.00000 0.03401 0.03856 = 0.03737 -0.00098 0.00222 0.00004 C43 1 0.486721 0.963955 0.585277 11.00000 0.05462 0.03995 = 0.05406 0.00138 0.00878 0.00200 AFIX 43 H43 2 0.496611 0.987835 0.552934 11.00000 -1.20000 AFIX 0 C44 1 0.450083 1.002572 0.631596 11.00000 0.05535 0.05270 = 0.07037 -0.01252 0.00851 0.01099 AFIX 43 H44 2 0.434869 1.052194 0.629820 11.00000 -1.20000 AFIX 0 C45 1 0.435328 0.969709 0.680537 11.00000 0.04090 0.08679 = 0.05333 -0.02114 0.00331 0.01033 C46 1 0.454775 0.895196 0.680867 11.00000 0.06415 0.09406 = 0.03898 0.00978 0.00899 0.01195 AFIX 43 H46 2 0.442486 0.871038 0.712874 11.00000 -1.20000 AFIX 0 C47 1 0.492182 0.855494 0.634641 11.00000 0.06127 0.05657 = 0.04210 0.01033 0.00641 0.01309 AFIX 43 H47 2 0.506023 0.805572 0.636082 11.00000 -1.20000 AFIX 0 C48 1 0.399437 1.013438 0.732383 11.00000 0.07832 0.14298 = 0.07674 -0.03774 0.01446 0.03378 AFIX 137 H48A 2 0.478934 1.043284 0.755812 11.00000 -1.50000 H48B 2 0.357091 0.978030 0.754414 11.00000 -1.50000 H48C 2 0.339596 1.046647 0.719701 11.00000 -1.50000 AFIX 0 F7 3 -0.212086 0.596545 0.261706 11.00000 0.05305 0.08986 = 0.07209 0.00424 0.02118 0.02011 F8 3 -0.226775 0.566719 0.170903 11.00000 0.03988 0.09386 = 0.05707 0.02491 -0.01012 0.00624 F9 3 -0.209245 0.481595 0.227480 11.00000 0.04635 0.06588 = 0.07572 0.01994 0.00411 -0.00706 O3 5 0.030533 0.551196 0.284040 11.00000 0.03907 0.04589 = 0.03288 0.00889 -0.00187 0.00303 N5 4 0.210323 0.650962 0.288782 11.00000 0.03630 0.04136 = 0.03294 0.00205 0.00062 0.00570 N6 4 0.015795 0.654531 0.225529 11.00000 0.04300 0.04234 = 0.03972 0.00785 0.00063 0.00765 C49 1 0.128486 0.687627 0.254352 11.00000 0.04601 0.03540 = 0.03872 0.00582 0.00510 0.00685 AFIX 43 H49 2 0.156798 0.739045 0.252009 11.00000 -1.20000 AFIX 0 C50 1 0.158191 0.582885 0.307120 11.00000 0.03556 0.03994 = 0.02772 0.00041 0.00441 0.00751 C51 1 0.244944 0.563802 0.349844 11.00000 0.03903 0.04366 = 0.02970 -0.00512 0.00043 0.01587 C52 1 0.361895 0.623868 0.359160 11.00000 0.03785 0.04661 = 0.03549 -0.00925 0.00186 0.01362 C53 1 0.337712 0.677872 0.321315 11.00000 0.03556 0.04516 = 0.03676 -0.00795 0.00581 0.00906 C54 1 0.430605 0.740696 0.317179 11.00000 0.04748 0.05146 = 0.05388 -0.00672 0.01299 0.00075 AFIX 43 H54 2 0.411483 0.775032 0.291619 11.00000 -1.20000 AFIX 0 C55 1 0.553402 0.750341 0.352726 11.00000 0.04351 0.06782 = 0.07384 -0.01677 0.00679 -0.00256 AFIX 43 H55 2 0.618306 0.792337 0.351496 11.00000 -1.20000 AFIX 0 C56 1 0.581131 0.698206 0.390221 11.00000 0.03926 0.08150 = 0.06946 -0.02143 -0.01091 0.01300 AFIX 43 H56 2 0.664651 0.705910 0.413565 11.00000 -1.20000 AFIX 0 C57 1 0.488054 0.635368 0.393710 11.00000 0.04527 0.06046 = 0.04996 -0.00870 -0.00672 0.01795 AFIX 43 H57 2 0.508953 0.600844 0.418857 11.00000 -1.20000 AFIX 0 C58 1 0.224552 0.497005 0.381206 11.00000 0.04167 0.04429 = 0.03192 -0.00010 0.00504 0.02101 C59 1 0.275696 0.503978 0.440110 11.00000 0.07210 0.05606 = 0.03618 -0.00205 0.00244 0.02845 AFIX 43 H59 2 0.321010 0.551137 0.459359 11.00000 -1.20000 AFIX 0 C60 1 0.260011 0.442123 0.470045 11.00000 0.08882 0.07210 = 0.03952 0.01397 0.01001 0.03791 AFIX 43 H60 2 0.294075 0.447888 0.509187 11.00000 -1.20000 AFIX 0 C61 1 0.193697 0.371589 0.441897 11.00000 0.07621 0.06556 = 0.06079 0.02420 0.02261 0.03094 AFIX 43 H61 2 0.183583 0.329614 0.461821 11.00000 -1.20000 AFIX 0 C62 1 0.143174 0.364168 0.384517 11.00000 0.07174 0.05399 = 0.06178 0.00924 0.00954 0.01221 AFIX 43 H62 2 0.098305 0.316796 0.365494 11.00000 -1.20000 AFIX 0 C63 1 0.157655 0.425852 0.354325 11.00000 0.05387 0.05588 = 0.04133 0.00303 -0.00001 0.01070 AFIX 43 H63 2 0.121912 0.419500 0.315326 11.00000 -1.20000 AFIX 0 C64 1 -0.015138 0.573348 0.227771 11.00000 0.03615 0.04010 = 0.02997 0.00815 -0.00297 0.00489 C65 1 -0.167583 0.553854 0.222058 11.00000 0.04069 0.05412 = 0.04391 0.01315 0.00381 0.00798 C66 1 0.031707 0.526570 0.180401 11.00000 0.03112 0.04720 = 0.03456 0.00101 -0.00438 0.00537 C67 1 0.038314 0.450406 0.183516 11.00000 0.05611 0.04750 = 0.05298 -0.00165 -0.00495 0.00882 AFIX 43 H67 2 0.018802 0.428399 0.215602 11.00000 -1.20000 AFIX 0 C68 1 0.074364 0.406773 0.138326 11.00000 0.05906 0.05548 = 0.08313 -0.02061 -0.01477 0.01794 AFIX 43 H68 2 0.079126 0.355758 0.140992 11.00000 -1.20000 AFIX 0 C69 1 0.103136 0.437066 0.089831 11.00000 0.04182 0.08863 = 0.06158 -0.02286 -0.00170 0.01477 C70 1 0.097950 0.512637 0.087673 11.00000 0.05479 0.10089 = 0.04904 -0.00162 0.01367 0.01529 AFIX 43 H70 2 0.118645 0.534489 0.055689 11.00000 -1.20000 AFIX 0 C71 1 0.062525 0.557735 0.132062 11.00000 0.04719 0.06340 = 0.04710 0.00326 0.00621 0.00941 AFIX 43 H71 2 0.059485 0.608925 0.129338 11.00000 -1.20000 AFIX 0 C72 1 0.136011 0.387478 0.040467 11.00000 0.07446 0.14187 = 0.10038 -0.05118 0.01357 0.02968 AFIX 137 H72A 2 0.181015 0.348666 0.055097 11.00000 -1.50000 H72B 2 0.192711 0.418404 0.020285 11.00000 -1.50000 H72C 2 0.055185 0.363871 0.014670 11.00000 -1.50000 AFIX 0 F10 3 -0.220330 0.427873 0.057082 11.00000 0.04397 0.05752 = 0.09941 0.00183 0.00360 -0.01480 F11 3 -0.238899 0.319576 0.005646 11.00000 0.05182 0.09602 = 0.09578 -0.01801 0.02401 0.01038 F12 3 -0.238558 0.324366 0.095889 11.00000 0.04540 0.07487 = 0.08652 0.01665 -0.01009 0.01035 O4 5 -0.482040 0.268500 0.035733 11.00000 0.03628 0.03051 = 0.04815 0.00488 -0.00214 0.00207 N7 4 -0.657172 0.287932 -0.033544 11.00000 0.03604 0.02830 = 0.03674 0.00668 0.00427 0.00172 N8 4 -0.465771 0.380621 -0.014919 11.00000 0.04802 0.03594 = 0.04257 0.00603 0.00694 -0.00506 C73 1 -0.576525 0.349266 -0.046298 11.00000 0.04523 0.03218 = 0.03456 0.00593 0.00716 0.00177 AFIX 43 H73 2 -0.603885 0.369364 -0.079799 11.00000 -1.20000 AFIX 0 C74 1 -0.611338 0.247191 0.010101 11.00000 0.03418 0.02912 = 0.03371 0.00486 0.00304 0.00577 C75 1 -0.704448 0.186782 0.014563 11.00000 0.03571 0.03006 = 0.03084 0.00258 0.00666 0.00551 C76 1 -0.818316 0.188385 -0.029912 11.00000 0.03574 0.03109 = 0.02814 0.00104 0.00628 0.00436 C77 1 -0.786728 0.251317 -0.059173 11.00000 0.03393 0.03002 = 0.03194 0.00150 0.00395 0.00364 C78 1 -0.874393 0.270920 -0.102823 11.00000 0.04735 0.03761 = 0.03582 0.00912 0.00405 0.00475 AFIX 43 H78 2 -0.851582 0.313616 -0.120792 11.00000 -1.20000 AFIX 0 C79 1 -0.997316 0.224262 -0.118534 11.00000 0.04648 0.05822 = 0.03794 0.01167 -0.00488 0.00704 AFIX 43 H79 2 -1.058428 0.234860 -0.148476 11.00000 -1.20000 AFIX 0 C80 1 -1.031781 0.161963 -0.090710 11.00000 0.03897 0.05599 = 0.04762 0.00830 0.00067 -0.00084 AFIX 43 H80 2 -1.116042 0.131908 -0.102083 11.00000 -1.20000 AFIX 0 C81 1 -0.944215 0.143261 -0.046461 11.00000 0.03946 0.04032 = 0.04024 0.00659 0.00650 -0.00133 AFIX 43 H81 2 -0.968966 0.101263 -0.028061 11.00000 -1.20000 AFIX 0 C82 1 -0.694371 0.129339 0.054578 11.00000 0.03198 0.03722 = 0.03510 0.00937 0.00694 0.00339 C83 1 -0.658631 0.150571 0.113367 11.00000 0.06544 0.05090 = 0.03808 0.00470 0.00178 0.00480 AFIX 43 H83 2 -0.638386 0.202109 0.128204 11.00000 -1.20000 AFIX 0 C84 1 -0.652668 0.095546 0.150549 11.00000 0.08236 0.07682 = 0.03760 0.01831 -0.00042 0.01028 AFIX 43 H84 2 -0.628643 0.110564 0.189982 11.00000 -1.20000 AFIX 0 C85 1 -0.681731 0.020151 0.129531 11.00000 0.06115 0.06205 = 0.06503 0.03457 0.00768 0.00895 AFIX 43 H85 2 -0.677793 -0.016458 0.154469 11.00000 -1.20000 AFIX 0 C86 1 -0.717074 -0.001949 0.071142 11.00000 0.06054 0.04057 = 0.06064 0.01496 0.00680 0.00066 AFIX 43 H86 2 -0.736750 -0.053607 0.056653 11.00000 -1.20000 AFIX 0 C87 1 -0.723429 0.052102 0.034077 11.00000 0.05594 0.03821 = 0.04244 0.00700 0.00716 0.00399 AFIX 43 H87 2 -0.747586 0.036483 -0.005282 11.00000 -1.20000 AFIX 0 C88 1 -0.432870 0.350310 0.038573 11.00000 0.03724 0.03031 = 0.04407 0.00291 0.00245 -0.00325 C89 1 -0.280535 0.355535 0.049470 11.00000 0.04013 0.04932 = 0.06786 0.00204 0.00764 -0.00118 C90 1 -0.477643 0.394038 0.088298 11.00000 0.03126 0.03522 = 0.03811 0.00309 -0.00155 -0.00193 C91 1 -0.478723 0.364476 0.139781 11.00000 0.05330 0.04369 = 0.04373 0.00525 -0.00458 0.00659 AFIX 43 H91 2 -0.453009 0.317552 0.143877 11.00000 -1.20000 AFIX 0 C92 1 -0.518180 0.404830 0.185336 11.00000 0.05773 0.06930 = 0.04032 0.00943 0.00008 0.00448 AFIX 43 H92 2 -0.519825 0.383961 0.219470 11.00000 -1.20000 AFIX 0 C93 1 -0.554919 0.475046 0.181097 11.00000 0.03392 0.06506 = 0.05099 -0.00609 0.00311 0.00490 C94 1 -0.553888 0.502984 0.129336 11.00000 0.04639 0.04637 = 0.05963 0.00049 0.00633 0.01027 AFIX 43 H94 2 -0.580046 0.549764 0.125093 11.00000 -1.20000 AFIX 0 C95 1 -0.515379 0.463848 0.083732 11.00000 0.04513 0.03912 = 0.04711 0.00607 0.00455 0.00281 AFIX 43 H95 2 -0.514837 0.484719 0.049552 11.00000 -1.20000 AFIX 0 C96 1 -0.594783 0.519437 0.231065 11.00000 0.06668 0.11300 = 0.06220 -0.01708 0.01254 0.02952 AFIX 137 H96A 2 -0.517063 0.551235 0.254377 11.00000 -1.50000 H96B 2 -0.636078 0.484530 0.253730 11.00000 -1.50000 H96C 2 -0.656584 0.550802 0.216893 11.00000 -1.50000 AFIX 0 O5 5 0.982148 0.743835 0.748614 11.00000 0.14952 0.16686 = 0.13370 -0.02446 0.00875 0.01943 PART 1 C97 1 1.206654 0.733322 0.751274 11.00000 0.17769 0.18425 = 0.19984 0.02711 0.02051 0.04380 AFIX 137 H97A 2 1.209961 0.737600 0.711610 11.00000 -1.50000 H97B 2 1.188375 0.680342 0.756252 11.00000 -1.50000 H97C 2 1.290794 0.757088 0.774535 11.00000 -1.50000 AFIX 0 C98 1 1.107194 0.769177 0.767703 11.00000 0.17581 0.16770 = 0.18494 0.01177 -0.01604 0.02069 AFIX 23 H98A 2 1.119434 0.772893 0.809258 11.00000 -1.20000 H98B 2 1.125295 0.821027 0.758669 11.00000 -1.20000 AFIX 0 PART 0 PART 2 C99 1 0.879964 0.775538 0.763206 11.00000 0.17264 0.15174 = 0.16168 -0.02781 0.01276 0.02334 AFIX 23 H99A 2 0.887652 0.777775 0.804555 11.00000 -1.20000 H99B 2 0.895030 0.827936 0.755114 11.00000 -1.20000 AFIX 0 C100 1 0.752010 0.745215 0.740046 11.00000 0.18535 0.21650 = 0.18656 -0.04979 0.05462 0.03619 AFIX 137 H10A 2 0.748471 0.715897 0.703455 11.00000 -1.50000 H10B 2 0.701805 0.785536 0.734987 11.00000 -1.50000 H10C 2 0.714727 0.712641 0.765218 11.00000 -1.50000 AFIX 0 HKLF 4 REM 01_a.res in P-1 REM R1 = 0.0729 for 9757 Fo > 4sig(Fo) and 0.1776 for all 20924 data REM 1132 parameters refined using 105 restraints END WGHT 0.0967 1.2342 REM Highest difference peak 0.428, deepest hole -0.459, 1-sigma level 0.136 Q1 1 0.0812 0.3194 0.0393 11.00000 0.05 0.43 Q2 1 0.2237 0.3724 0.0522 11.00000 0.05 0.41 Q3 1 -0.6031 0.4289 0.1822 11.00000 0.05 0.40 Q4 1 -0.6013 0.4778 0.1508 11.00000 0.05 0.40 Q5 1 1.1011 0.8389 0.5752 11.00000 0.05 0.39 Q6 1 -1.1484 0.1578 -0.0761 11.00000 0.05 0.39 Q7 1 0.4442 1.0044 0.7721 11.00000 0.05 0.38 Q8 1 1.0590 0.8115 0.5369 11.00000 0.05 0.38 Q9 1 1.1289 0.8987 0.5323 11.00000 0.05 0.38 Q10 1 -0.1491 0.6555 0.4064 11.00000 0.05 0.38 Q11 1 1.0513 0.7956 0.5615 11.00000 0.05 0.37 Q12 1 0.3938 0.9325 0.6858 11.00000 0.05 0.37 Q13 1 0.1212 0.3185 0.0844 11.00000 0.05 0.37 Q14 1 0.3928 0.9763 0.6541 11.00000 0.05 0.36 Q15 1 -0.5494 0.5108 0.2711 11.00000 0.05 0.36 Q16 1 0.1428 0.2851 0.0508 11.00000 0.05 0.36 Q17 1 0.0621 0.2517 0.0285 11.00000 0.05 0.35 Q18 1 1.2068 0.8690 0.5544 11.00000 0.05 0.35 Q19 1 0.2593 0.3644 0.1403 11.00000 0.05 0.34 Q20 1 0.0497 0.2872 0.0574 11.00000 0.05 0.34 REM The information below was added by Olex2. REM REM R1 = 0.0729 for 9757 Fo > 4sig(Fo) and 0.1776 for all 83277 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.43, deepest hole -0.46 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1776 REM R1_gt = 0.0729 REM wR_ref = 0.2102 REM GOOF = 1.041 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 83277 REM Reflections_gt = 9757 REM Parameters = n/a REM Hole = -0.46 REM Peak = 0.43 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received'